9-Triptycyldiphenylphosphine oxide

Base Information

• Chemical Name: 9-Triptycyldiphenylphosphine oxide
• CAS No.: 92012-53-8
• Molecular Formula: C₃₂H₂₃OP
• Molecular Weight: 454.508
• Mol file: 92012-53-8.mol

Synonyms:9-Triptycyldiphenylphosphine oxide

Chemical Property of 9-Triptycyldiphenylphosphine oxide

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 9-Triptycyldiphenylphosphine oxide

There total 2 articles about 9-Triptycyldiphenylphosphine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

9-bromotriptycene (15364-55-3) + diphenylphosphide ion (34676-89-6) → triptycene (477-75-8) + 9-Triptycyldiphenylphosphine oxide (92012-53-8)

Guidance literature:

In ammonia; for 5.83333h; Product distribution; Irradiation; other nucleophile, other triptycene;

DOI:10.1021/jo00198a007

Reference yield:

9-bromotriptycene (15364-55-3) + triphenylphosphine (603-35-0) → 9-Triptycyldiphenylphosphine oxide (92012-53-8)

Guidance literature:

With sodium; tert-butyl alcohol; Multistep reaction; 1) ammonia 2) irradiation 350 min;

DOI:10.1021/jo00198a007

upstream raw materials:

9-bromotriptycene

diphenylphosphide ion

triphenylphosphine