Technology Process of 2-(m-ethoxyphenyl)-5,6-dihydro-pyrazolo-<5,1-a>isoquinoline
There total 7 articles about 2-(m-ethoxyphenyl)-5,6-dihydro-pyrazolo-<5,1-a>isoquinoline which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium;
In
ethanol;
1.) 1 h, room temp.; 2.) 60 deg C, 20 h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: p-toluenesulfonic acid / benzene / 1 h / Heating
2: potassium t-butoxide / 2-methyl-propan-2-ol / 5 h / Heating
3: 85 percent / 98percent H2SO4 / ethanol / 11 h / Heating
4: 90 percent / hydrogen / 10percent palladium on carbon / methanol / 6 h / 760 Torr / Ambient temperature
5: 87 percent / sodium / ethanol / 1.) 1 h, room temp.; 2.) 60 deg C, 20 h
With
sulfuric acid; potassium tert-butylate; hydrogen; sodium;
palladium on activated charcoal; toluene-4-sulfonic acid;
In
methanol; ethanol; tert-butyl alcohol; benzene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: p-toluenesulfonic acid / benzene / 1 h / Heating
2: potassium t-butoxide / 2-methyl-propan-2-ol / 5 h / Heating
3: 85 percent / 98percent H2SO4 / ethanol / 11 h / Heating
4: 90 percent / hydrogen / 10percent palladium on carbon / methanol / 6 h / 760 Torr / Ambient temperature
5: 87 percent / sodium / ethanol / 1.) 1 h, room temp.; 2.) 60 deg C, 20 h
With
sulfuric acid; potassium tert-butylate; hydrogen; sodium;
palladium on activated charcoal; toluene-4-sulfonic acid;
In
methanol; ethanol; tert-butyl alcohol; benzene;
