Technology Process of exosensor 517
There total 4 articles about exosensor 517 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0);
In
tetrahydrofuran;
DOI:10.1021/cn400128s
- Guidance literature:
-
Multi-step reaction with 4 steps
1: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate
2: boron tribromide / dichloromethane
3: N-ethyl-N,N-diisopropylamine / tetrahydrofuran
4: tris-(dibenzylideneacetone)dipalladium(0); dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate / tetrahydrofuran
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); boron tribromide; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; dichloromethane;
1: |Suzuki Coupling / 4: |Buchwald-Hartwig Coupling;
DOI:10.1021/cn400128s
- Guidance literature:
-
Multi-step reaction with 4 steps
1: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate
2: boron tribromide / dichloromethane
3: N-ethyl-N,N-diisopropylamine / tetrahydrofuran
4: tris-(dibenzylideneacetone)dipalladium(0); dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate / tetrahydrofuran
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); boron tribromide; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; dichloromethane;
1: |Suzuki Coupling / 4: |Buchwald-Hartwig Coupling;
DOI:10.1021/cn400128s
