N,N'-dimethyl-N-[4-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-3-nitrobenzyl-oxycarbonyl]-ethylenediamine hydrochloride

Base Information

• Chemical Name: N,N'-dimethyl-N-[4-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-3-nitrobenzyl-oxycarbonyl]-ethylenediamine hydrochloride
• CAS No.: 1224946-43-3
• Molecular Formula: C₂₆H₃₅N₃O₁₄*ClH
• Molecular Weight: 650.037

Synonyms:N,N'-dimethyl-N-[4-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-3-nitrobenzyl-oxycarbonyl]-ethylenediamine hydrochloride

Chemical Property of N,N'-dimethyl-N-[4-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-3-nitrobenzyl-oxycarbonyl]-ethylenediamine hydrochloride

Chemical Property:

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Technology Process of N,N'-dimethyl-N-[4-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-3-nitrobenzyl-oxycarbonyl]-ethylenediamine hydrochloride

There total 1 articles about N,N'-dimethyl-N-[4-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-3-nitrobenzyl-oxycarbonyl]-ethylenediamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N'-dimethyl-N-[4-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-3-nitrobenzyl-oxycarbonyl]-N'-(tert-butyloxycarbonyl)-ethylenediamine (1224946-42-2) → N,N'-dimethyl-N-[4-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-3-nitrobenzyl-oxycarbonyl]-ethylenediamine hydrochloride (1224946-43-3)

Guidance literature:

With hydrogenchloride; In ethyl acetate; at 0 - 25 ℃; for 0.5h; Inert atmosphere;

DOI:10.1039/b925070k

Reference yield: 98.0%

N,N'-dimethyl-N-[4-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-3-nitrobenzyl-oxycarbonyl]-ethylenediamine hydrochloride (1224946-43-3) + 4-Nitrophenyl chloroformate (7693-46-1) → C33H38N4O17

Guidance literature:

With pyridine; In dichloromethane; at 0 ℃; Inert atmosphere;

DOI:10.1039/b925070k

Reference yield: 97.0%

phosgene (75-44-5) + N,N'-dimethyl-N-[4-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-3-nitrobenzyl-oxycarbonyl]-ethylenediamine hydrochloride (1224946-43-3) → C27H34ClN3O15 (1224946-47-7)

Guidance literature:

With triethylamine; In dichloromethane; toluene; at 0 ℃; Inert atmosphere;

DOI:10.1039/b925070k

upstream raw materials:

N,N'-dimethyl-N-[4-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-3-nitrobenzyl-oxycarbonyl]-N'-(tert-butyloxycarbonyl)-ethylenediamine

Downstream raw materials:

C₂₇H₃₄ClN₃O₁₅

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