Methyl (3S)-3-[4-(tert-butyldimethylsilyloxy)phenyl]-3-hydroxypropionate

Base Information

Chemical Name:Methyl (3S)-3-[4-(tert-butyldimethylsilyloxy)phenyl]-3-hydroxypropionate
CAS No.:1202577-54-5
Molecular Formula:C₁₆H₂₆O₄Si
Molecular Weight:310.466
Hs Code.:

Synonyms:Methyl (3S)-3-[4-(tert-butyldimethylsilyloxy)phenyl]-3-hydroxypropionate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl (3S)-3-[4-(tert-butyldimethylsilyloxy)phenyl]-3-hydroxypropionate

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Technology Process of Methyl (3S)-3-[4-(tert-butyldimethylsilyloxy)phenyl]-3-hydroxypropionate

There total 1 articles about Methyl (3S)-3-[4-(tert-butyldimethylsilyloxy)phenyl]-3-hydroxypropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 501334-19-6
methyl 3-[4-(tert-butyldimethylsilyloxybenzyl)phenyl]-3-oxopropanoate

: 1202577-54-5
Methyl (3S)-3-[4-(tert-butyldimethylsilyloxy)phenyl]-3-hydroxypropionate

Guidance literature:: With formic acid; triethylamine; Noyori's catalyst; at 0 - 35 ℃; Inert atmosphere;

Reference yield: 74.0%

: 1202577-54-5
Methyl (3S)-3-[4-(tert-butyldimethylsilyloxy)phenyl]-3-hydroxypropionate

: 75-03-6
ethyl iodide

: 1202577-55-6
methyl (3S)-3-[4-(tert-butyldimethylsilyloxy)phenyl]-3-ethoxypropanoate

Guidance literature:: With silver(l) oxide; In toluene; at 20 - 110 ℃; Inert atmosphere;

Reference yield:

: 1202577-54-5
Methyl (3S)-3-[4-(tert-butyldimethylsilyloxy)phenyl]-3-hydroxypropionate

: 1202575-57-2
(3S)-3-[4-(2,3-dihydro-1H-inden-2-yloxy)phenyl]-3-ethoxypropanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: silver(l) oxide / toluene / 20 - 110 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / 0 °C

3: toluene; tetrahydrofuran / 20 - 50 °C / Inert atmosphere

4: sodium hydroxide; water / ethanol; tetrahydrofuran / 4 h / 20 °C

With tetrabutyl ammonium fluoride; water; sodium hydroxide; silver(l) oxide; In tetrahydrofuran; ethanol; toluene;