C₄₂H₃₆N₄O₆

Base Information

• Chemical Name: C₄₂H₃₆N₄O₆
• CAS No.: 195617-13-1
• Molecular Formula: C₄₂H₃₆N₄O₆
• Molecular Weight: 692.771
• Mol file: 195617-13-1.mol

Synonyms:C₄₂H₃₆N₄O₆

Chemical Property of C₄₂H₃₆N₄O₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₂H₃₆N₄O₆

There total 4 articles about C₄₂H₃₆N₄O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

O-benzylhydoxylamine hydrochloride (2687-43-6) + C35H29N3O6 (188027-88-5) → C42H36N4O6 (195617-13-1)

Guidance literature:

With sodium acetate; In ethanol; for 0.5h; Heating;

DOI:10.1021/ja971304x

Reference yield:

C36H31N3O7 (188028-91-3) → C42H36N4O6 (195617-13-1)

Guidance literature:

Multi-step reaction with 4 steps

1: 89 percent / LiBH₄ / tetrahydrofuran / 0.33 h

2: 71 percent / pyridinium trifluoroacetate, 1,3-dicyclohexylcarbodiimide / benzene; dimethylsulfoxide / 9 h / Ambient temperature

3: 85 percent / BF₃*OEt₂ / diethyl ether / 24 h / 25 - 30 °C

4: 85 percent / NaOAc / aq. ethanol / 0.5 h / Heating

With lithium borohydride; boron trifluoride diethyl etherate; sodium acetate; pyridinium trifluroacetate; dicyclohexyl-carbodiimide; In tetrahydrofuran; diethyl ether; ethanol; dimethyl sulfoxide; benzene;

DOI:10.1021/ja971304x

Reference yield:

C35H29N3O6 (188027-84-1) → C42H36N4O6 (195617-13-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 85 percent / BF₃*OEt₂ / diethyl ether / 24 h / 25 - 30 °C

2: 85 percent / NaOAc / aq. ethanol / 0.5 h / Heating

With boron trifluoride diethyl etherate; sodium acetate; In diethyl ether; ethanol;

DOI:10.1021/ja971304x

upstream raw materials:

O-benzylhydoxylamine hydrochloride

C₃₅H₂₉N₃O₆

C₃₆H₃₁N₃O₇

C₃₅H₃₁N₃O₆

Downstream raw materials:

C₃₄H₂₈N₄O₄

TAN-1030A

C₄₃H₃₈N₄O₆