2-{4-[3-(tert-butyl-dimethyl-silanyloxy)-propyl]-phenyl}-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

Base Information

Chemical Name:2-{4-[3-(tert-butyl-dimethyl-silanyloxy)-propyl]-phenyl}-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane
CAS No.:936023-12-0
Molecular Formula:C₂₁H₃₇BO₃Si
Molecular Weight:376.419
Hs Code.:

Synonyms:2-{4-[3-(tert-butyl-dimethyl-silanyloxy)-propyl]-phenyl}-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

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Chemical Property of 2-{4-[3-(tert-butyl-dimethyl-silanyloxy)-propyl]-phenyl}-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

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Technology Process of 2-{4-[3-(tert-butyl-dimethyl-silanyloxy)-propyl]-phenyl}-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

There total 4 articles about 2-{4-[3-(tert-butyl-dimethyl-silanyloxy)-propyl]-phenyl}-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 153993-80-7
[3-(4-bromophenyl)propoxy](tert-butyl)dimethylsilane

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 936023-12-0
2-{4-[3-(tert-butyl-dimethyl-silanyloxy)-propyl]-phenyl}-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

Guidance literature:: With triethylamine; bis-triphenylphosphine-palladium(II) chloride; In 1,4-dioxane; at 100 ℃; for 16h;

Reference yield:

: 153993-80-7
[3-(4-bromophenyl)propoxy](tert-butyl)dimethylsilane

: 73183-34-3
bis(pinacol)diborane

: 936023-12-0
2-{4-[3-(tert-butyl-dimethyl-silanyloxy)-propyl]-phenyl}-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

Guidance literature:: With potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1,4-dioxane; at 80 ℃; for 3h; Inert atmosphere;

Reference yield:

: 1643-30-7
3-(4-bromophenyl)propionic acid

: 936023-12-0
2-{4-[3-(tert-butyl-dimethyl-silanyloxy)-propyl]-phenyl}-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 5 h / 0 °C / Reflux; Inert atmosphere

1.2: 0 °C / Inert atmosphere

2.1: dmap; triethylamine / dichloromethane / 17 - 25 °C / Inert atmosphere

3.1: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 3 h / 80 °C / Inert atmosphere

With dmap; lithium aluminium tetrahydride; potassium acetate; triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; 1,4-dioxane; dichloromethane;