trans-N-(benzyloxycarbonyl)cyclobutanamine-3-acetaldehyde diethyl acetal

Base Information

Chemical Name:trans-N-(benzyloxycarbonyl)cyclobutanamine-3-acetaldehyde diethyl acetal
CAS No.:171549-99-8
Molecular Formula:C₁₈H₂₇NO₄
Molecular Weight:321.417
Hs Code.:

Synonyms:trans-N-(benzyloxycarbonyl)cyclobutanamine-3-acetaldehyde diethyl acetal

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Chemical Property of trans-N-(benzyloxycarbonyl)cyclobutanamine-3-acetaldehyde diethyl acetal

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Technology Process of trans-N-(benzyloxycarbonyl)cyclobutanamine-3-acetaldehyde diethyl acetal

There total 4 articles about trans-N-(benzyloxycarbonyl)cyclobutanamine-3-acetaldehyde diethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 104-15-4
toluene-4-sulfonic acid

: 122-51-0
orthoformic acid triethyl ester

: 171549-94-3
trans-N-(benzyloxycarbonyl)cyclobutanamine-3-acetaldehyde

: 171549-99-8
trans-N-(benzyloxycarbonyl)cyclobutanamine-3-acetaldehyde diethyl acetal

Guidance literature:: In ethanol;

Reference yield: 94.0%

: 122-51-0
orthoformic acid triethyl ester

: 171549-94-3
trans-N-(benzyloxycarbonyl)cyclobutanamine-3-acetaldehyde

: 171549-99-8
trans-N-(benzyloxycarbonyl)cyclobutanamine-3-acetaldehyde diethyl acetal

Guidance literature:: With toluene-4-sulfonic acid; In ethanol; for 3h; Heating;
DOI:10.1021/jm000956k

Reference yield:

: 1-Isocyanato-3-methylene-cyclobutane

: 171549-99-8
trans-N-(benzyloxycarbonyl)cyclobutanamine-3-acetaldehyde diethyl acetal

Guidance literature:: Multi-step reaction with 3 steps

1: DPPA

2: 19.5 percent / H₂; (Ph₃P)3RhCl / toluene / 18 h / 70 °C / 76000 Torr

3: 94 percent / pTsOH / ethanol / 3 h / Heating

With Wilkinson's catalyst; diphenyl-phosphinic acid; hydrogen; toluene-4-sulfonic acid; In ethanol; toluene;
DOI:10.1021/jm000956k