methyl 4-pent-4-enoylbenzoate

Base Information

Chemical Name:methyl 4-pent-4-enoylbenzoate
CAS No.:1363415-73-9
Molecular Formula:C₁₃H₁₄O₃
Molecular Weight:218.252
Hs Code.:

Synonyms:methyl 4-pent-4-enoylbenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 4-pent-4-enoylbenzoate

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Technology Process of methyl 4-pent-4-enoylbenzoate

There total 4 articles about methyl 4-pent-4-enoylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 925198-15-8
C₁₂H₁₃NO₃

: 7103-09-5
4-but-1-enylmagnesium bromide

: 1363415-73-9
methyl 4-pent-4-enoylbenzoate

Guidance literature:: C₁₂H₁₃NO₃; With 2-fluoropyridine; trifluoromethylsulfonic anhydride; In dichloromethane; at -78 - 0 ℃; Inert atmosphere;

4-but-1-enylmagnesium bromide; In dichloromethane; at 0 ℃; for 0.416667h; Inert atmosphere;

With hydrogenchloride; water; In tetrahydrofuran; dichloromethane; at 65 ℃; for 2h; chemoselective reaction; Inert atmosphere;
DOI:10.1038/nchem.1268

Reference yield: 40.0%

: 52540-22-4
methyl 4-(2-chloroacetyl)benzoate

: 107-18-6
allyl alcohol

: 1363415-73-9
methyl 4-pent-4-enoylbenzoate

Guidance literature:: With tributyl-amine; palladium diacetate; trifluoperazine dihydrochloride; In toluene; at 130 ℃; for 2h; under 15001.5 Torr; Gas phase;
DOI:10.1039/c2cc32391e