(2R,3R)-N,N,N',N'-tetramethyl-2-benzyloxy-3-(2-tosyloxy)ethoxysuccinamide

Base Information

Chemical Name:(2R,3R)-N,N,N',N'-tetramethyl-2-benzyloxy-3-(2-tosyloxy)ethoxysuccinamide
CAS No.:117036-87-0
Molecular Formula:C₂₄H₃₂N₂O₇S
Molecular Weight:492.593
Hs Code.:

Synonyms:(2R,3R)-N,N,N',N'-tetramethyl-2-benzyloxy-3-(2-tosyloxy)ethoxysuccinamide

Suppliers and Price of (2R,3R)-N,N,N',N'-tetramethyl-2-benzyloxy-3-(2-tosyloxy)ethoxysuccinamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3R)-N,N,N',N'-tetramethyl-2-benzyloxy-3-(2-tosyloxy)ethoxysuccinamide

Chemical Property:

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Technology Process of (2R,3R)-N,N,N',N'-tetramethyl-2-benzyloxy-3-(2-tosyloxy)ethoxysuccinamide

There total 5 articles about (2R,3R)-N,N,N',N'-tetramethyl-2-benzyloxy-3-(2-tosyloxy)ethoxysuccinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 117034-04-5
(2R,3R)-N,N,N',N'-tetramethyl-2-benzyloxy-3-(2-hydroxy)ethoxysuccinamide

: 98-59-9
p-toluenesulfonyl chloride

: 117036-87-0
(2R,3R)-N,N,N',N'-tetramethyl-2-benzyloxy-3-(2-tosyloxy)ethoxysuccinamide

Guidance literature:: With triethylamine; In dichloromethane;

Reference yield:

: 26549-65-5
N,N,N',N'-tetramethyl L-tartramide

: 117036-87-0
(2R,3R)-N,N,N',N'-tetramethyl-2-benzyloxy-3-(2-tosyloxy)ethoxysuccinamide

Guidance literature:: Multi-step reaction with 4 steps

1: 64 percent / sodium hydride / dimethylformamide / 7 h / 80 °C

2: thallous ethoxide / dimethylformamide / 15 h / 60 °C

3: 100 percent / HCl / methanol / 1.5 h / Heating

4: 78 percent / Et₃N / CH₂Cl₂

With hydrogenchloride; thallium (I) ethoxide; sodium hydride; triethylamine; In methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 100-39-0
benzyl bromide

: 117036-87-0
(2R,3R)-N,N,N',N'-tetramethyl-2-benzyloxy-3-(2-tosyloxy)ethoxysuccinamide

Guidance literature:: Multi-step reaction with 4 steps

1: 64 percent / sodium hydride / dimethylformamide / 7 h / 80 °C

2: thallous ethoxide / dimethylformamide / 15 h / 60 °C

3: 100 percent / HCl / methanol / 1.5 h / Heating

4: 78 percent / Et₃N / CH₂Cl₂

With hydrogenchloride; thallium (I) ethoxide; sodium hydride; triethylamine; In methanol; dichloromethane; N,N-dimethyl-formamide;