4-N-(4-imino-2-thioxo-1,3-thiazolidin-3-yl)-6-methyl-2-p-toluenesulfonylamidopyrimidine

Base Information

Chemical Name:4-N-(4-imino-2-thioxo-1,3-thiazolidin-3-yl)-6-methyl-2-p-toluenesulfonylamidopyrimidine
CAS No.:353302-94-0
Molecular Formula:C₁₅H₁₆N₆O₂S₃
Molecular Weight:408.529
Hs Code.:

Synonyms:4-N-(4-imino-2-thioxo-1,3-thiazolidin-3-yl)-6-methyl-2-p-toluenesulfonylamidopyrimidine

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Chemical Property of 4-N-(4-imino-2-thioxo-1,3-thiazolidin-3-yl)-6-methyl-2-p-toluenesulfonylamidopyrimidine

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Technology Process of 4-N-(4-imino-2-thioxo-1,3-thiazolidin-3-yl)-6-methyl-2-p-toluenesulfonylamidopyrimidine

There total 5 articles about 4-N-(4-imino-2-thioxo-1,3-thiazolidin-3-yl)-6-methyl-2-p-toluenesulfonylamidopyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 107-14-2
chloroacetonitrile

: C₁₃H₁₄N₅O₂S₃^(1-)*K⁽¹⁺⁾

: 353302-94-0
4-N-(4-imino-2-thioxo-1,3-thiazolidin-3-yl)-6-methyl-2-p-toluenesulfonylamidopyrimidine

Guidance literature:: In water; at 0 - 20 ℃;
DOI:10.1023/A:1017523602062

Reference yield:

: 7749-47-5
2-amino-6-methoxy-4-methylpyrimidine

: 353302-94-0
4-N-(4-imino-2-thioxo-1,3-thiazolidin-3-yl)-6-methyl-2-p-toluenesulfonylamidopyrimidine

Guidance literature:: Multi-step reaction with 4 steps

1: 51 percent / pyridine / 20 °C

2: 99 percent / H₂NNH₂*H₂O / dioxane / 100 - 110 °C

3: KOH / ethanol / 65 - 70 °C

4: 99 percent / H₂O / 0 - 20 °C

With potassium hydroxide; hydrazine hydrate; In 1,4-dioxane; pyridine; ethanol; water;
DOI:10.1023/A:1017523602062

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 353302-94-0
4-N-(4-imino-2-thioxo-1,3-thiazolidin-3-yl)-6-methyl-2-p-toluenesulfonylamidopyrimidine

Guidance literature:: Multi-step reaction with 4 steps

1: 51 percent / pyridine / 20 °C

2: 99 percent / H₂NNH₂*H₂O / dioxane / 100 - 110 °C

3: KOH / ethanol / 65 - 70 °C

4: 99 percent / H₂O / 0 - 20 °C

With potassium hydroxide; hydrazine hydrate; In 1,4-dioxane; pyridine; ethanol; water;
DOI:10.1023/A:1017523602062