C₁₀H₁₁BrFNO₂

Base Information

Chemical Name:C₁₀H₁₁BrFNO₂
CAS No.:880386-23-2
Molecular Formula:C₁₀H₁₁BrFNO₂
Molecular Weight:276.105
Hs Code.:

C<sub>10</sub>H<sub>11</sub>BrFNO<sub>2</sub>

Synonyms:C₁₀H₁₁BrFNO₂

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Chemical Property of C₁₀H₁₁BrFNO₂

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Technology Process of C₁₀H₁₁BrFNO₂

There total 7 articles about C₁₀H₁₁BrFNO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4-(3-bromo-4-fluorobenzylidene)-2-methyloxazol-5(4H)-one

: 880386-23-2
C₁₀H₁₁BrFNO₂

Guidance literature:: Multi-step reaction with 5 steps

1: water; acetic acid / 1 h / 100 °C

2: bis(1,5-cyclooctadiene)rhodium(I) trifluoromethanesulfonate; (R)-N-diphenylphosphino-N-methyl-1-[(S)-2-(diphenylphosphino)ferrocenyl]ethylamine; hydrogen / methanol / 24 h / 20 °C / 1551.49 Torr / Inert atmosphere

3: acylase "Amano" enzyme; water; cobalt(II) chloride; potassium hydroxide / 96 h / 40 °C / pH 8 / Enzymatic reaction

4: thionyl chloride

5: 16 h / 20 °C

With bis(1,5-cyclooctadiene)rhodium(I) trifluoromethanesulfonate; thionyl chloride; (R)-N-diphenylphosphino-N-methyl-1-[(S)-2-(diphenylphosphino)ferrocenyl]ethylamine; acylase "Amano" enzyme; water; hydrogen; acetic acid; cobalt(II) chloride; potassium hydroxide; In methanol;
DOI:10.1039/c0ob01004a

Reference yield:

: 2-acetylamino-3-(3-bromo-4-fluorophenyl)propionic acid

: 880386-23-2
C₁₀H₁₁BrFNO₂

Guidance literature:: Multi-step reaction with 4 steps

1: water; isopropyl alcohol / 20 - 70 °C / Resolution of racemate

2: acylase "Amano" enzyme; water; cobalt(II) chloride; potassium hydroxide / 96 h / 40 °C / pH 8 / Enzymatic reaction

3: thionyl chloride

4: 16 h / 20 °C

With thionyl chloride; acylase "Amano" enzyme; water; cobalt(II) chloride; potassium hydroxide; In water; isopropyl alcohol;
DOI:10.1039/c0ob01004a

Reference yield:

: 77771-02-9
3-bromo-4-fluorobenzaldehyde

: 880386-23-2
C₁₀H₁₁BrFNO₂

Guidance literature:: Multi-step reaction with 6 steps

1: sodium acetate; acetic anhydride / 10 h / 130 °C

2: water; acetic acid / 1 h / 100 °C

3: bis(1,5-cyclooctadiene)rhodium(I) trifluoromethanesulfonate; (R)-N-diphenylphosphino-N-methyl-1-[(S)-2-(diphenylphosphino)ferrocenyl]ethylamine; hydrogen / methanol / 24 h / 20 °C / 1551.49 Torr / Inert atmosphere

4: acylase "Amano" enzyme; water; cobalt(II) chloride; potassium hydroxide / 96 h / 40 °C / pH 8 / Enzymatic reaction

5: thionyl chloride

6: 16 h / 20 °C

With bis(1,5-cyclooctadiene)rhodium(I) trifluoromethanesulfonate; thionyl chloride; (R)-N-diphenylphosphino-N-methyl-1-[(S)-2-(diphenylphosphino)ferrocenyl]ethylamine; acylase "Amano" enzyme; water; hydrogen; sodium acetate; acetic anhydride; acetic acid; cobalt(II) chloride; potassium hydroxide; In methanol; 1: Erlenmeyer-Pl?chl azlactone synthesis;
DOI:10.1039/c0ob01004a