1-(3-formylphenyl)-N-(2-methoxybenzyl)-3-(trifluoromethyl)-1H-pyrazole-5-carboxamide

Base Information

Chemical Name:1-(3-formylphenyl)-N-(2-methoxybenzyl)-3-(trifluoromethyl)-1H-pyrazole-5-carboxamide
CAS No.:1051930-01-8
Molecular Formula:C₂₀H₁₆F₃N₃O₃
Molecular Weight:403.361
Hs Code.:

Synonyms:1-(3-formylphenyl)-N-(2-methoxybenzyl)-3-(trifluoromethyl)-1H-pyrazole-5-carboxamide

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Chemical Property of 1-(3-formylphenyl)-N-(2-methoxybenzyl)-3-(trifluoromethyl)-1H-pyrazole-5-carboxamide

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Technology Process of 1-(3-formylphenyl)-N-(2-methoxybenzyl)-3-(trifluoromethyl)-1H-pyrazole-5-carboxamide

There total 1 articles about 1-(3-formylphenyl)-N-(2-methoxybenzyl)-3-(trifluoromethyl)-1H-pyrazole-5-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1051930-00-7
1-(3-(1,3-dioxan-2-yl)phenyl)-N-(2-methoxybenzyl)-3-(trifluoromethyl)-1H-pyrazole-5-carboxamide

: 1051930-01-8
1-(3-formylphenyl)-N-(2-methoxybenzyl)-3-(trifluoromethyl)-1H-pyrazole-5-carboxamide

Guidance literature:: With water; acetic acid; at 90 ℃; for 2h;

Reference yield: 87.0%

: 1051930-01-8
1-(3-formylphenyl)-N-(2-methoxybenzyl)-3-(trifluoromethyl)-1H-pyrazole-5-carboxamide

: 75-16-1
methylmagnesium bromide

: 1051930-02-9
1-(3-(1-hydroxyethyl)phenyl)-N-(2-methoxybenzyl)-3-(trifluoromethyl)-1H-pyrazole-5-carboxamide

Guidance literature:: 1-(3-formylphenyl)-N-(2-methoxybenzyl)-3-(trifluoromethyl)-1H-pyrazole-5-carboxamide; methylmagnesium bromide; In tetrahydrofuran; at -78 - 0 ℃;

With water; In tetrahydrofuran;

Reference yield: 62.0%

: 1051930-01-8
1-(3-formylphenyl)-N-(2-methoxybenzyl)-3-(trifluoromethyl)-1H-pyrazole-5-carboxamide

: 57260-73-8
N-BOC-1,2-diaminoethane

: C₂₇H₃₂F₃N₅O₄

Guidance literature:: 1-(3-formylphenyl)-N-(2-methoxybenzyl)-3-(trifluoromethyl)-1H-pyrazole-5-carboxamide; N-BOC-1,2-diaminoethane; With acetic acid; In dichloromethane;

With sodium tris(acetoxy)borohydride; at 20 ℃; for 16h;
DOI:10.1016/j.bmcl.2009.09.110