tert-butylphenylphosphinic chlorosulfonic anhydride

Base Information

Chemical Name:tert-butylphenylphosphinic chlorosulfonic anhydride
CAS No.:97730-06-8
Molecular Formula:C₁₀H₁₄ClO₄PS
Molecular Weight:296.712
Hs Code.:

Synonyms:tert-butylphenylphosphinic chlorosulfonic anhydride

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Chemical Property of tert-butylphenylphosphinic chlorosulfonic anhydride

Chemical Property:

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Technology Process of tert-butylphenylphosphinic chlorosulfonic anhydride

There total 7 articles about tert-butylphenylphosphinic chlorosulfonic anhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 97730-04-6
tert-butylphenylphosphinic imidazolidosulfuric anhydride

: 75-36-5
acetyl chloride

: 2466-76-4
N-Acetylimidazole

: 97730-06-8
tert-butylphenylphosphinic chlorosulfonic anhydride

Guidance literature:: In diethyl ether; dichloromethane; for 1h; Yield given; Ambient temperature;

Reference yield:

: 82220-43-7,82220-48-2
tert-butylphenylphosphinic methanesulfonic anhydride

: 97730-06-8
tert-butylphenylphosphinic chlorosulfonic anhydride

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / acetone / 1 h / further educts: tert-butylphenylphosphinic trifluoromethanesulfonic, -imidazolidosulfuric, -4-methylbenzenesulfonic, -chlorsulfonic anhydrides

2: CH₂Cl₂; diethyl ether / 1 h / Ambient temperature

3: CH₂Cl₂; diethyl ether / 1 h / Ambient temperature

In diethyl ether; dichloromethane; acetone;

Reference yield:

: C₁₄H₂₆O₄PSSi⁽¹⁺⁾*I^(1-)

: 97730-06-8
tert-butylphenylphosphinic chlorosulfonic anhydride

Guidance literature:: Multi-step reaction with 6 steps

1: 2,6-lutidine / CH₂Cl₂ / 10 °C

2: CH₂Cl₂ / -80 °C

3: CH₂Cl₂ / 20 °C

4: CH₂Cl₂ / -80 °C

5: CH₂Cl₂; diethyl ether / 1 h / Ambient temperature

6: CH₂Cl₂; diethyl ether / 1 h / Ambient temperature

With 2,6-dimethylpyridine; In diethyl ether; dichloromethane;