6,6'-p-Phenylen-di-<2-oxo-4-phenyl-cyclohex-3-en-carbonsaeure-(1)-ethylester>

Base Information

• Chemical Name: 6,6'-p-Phenylen-di-<2-oxo-4-phenyl-cyclohex-3-en-carbonsaeure-(1)-ethylester>
• CAS No.: 96772-34-8
• Molecular Formula: C₃₆H₃₄O₆
• Molecular Weight: 562.662

Synonyms:6,6'-p-Phenylen-di-<2-oxo-4-phenyl-cyclohex-3-en-carbonsaeure-(1)-ethylester>

Chemical Property of 6,6'-p-Phenylen-di-<2-oxo-4-phenyl-cyclohex-3-en-carbonsaeure-(1)-ethylester>

Chemical Property:

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Technology Process of 6,6'-p-Phenylen-di-<2-oxo-4-phenyl-cyclohex-3-en-carbonsaeure-(1)-ethylester>

There total 3 articles about 6,6'-p-Phenylen-di-<2-oxo-4-phenyl-cyclohex-3-en-carbonsaeure-(1)-ethylester> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

1,4-bis-(3-oxo-3-phenyl-propenyl)-benzene (24915-93-3,3251-38-5) + ethyl acetoacetate (141-97-9) → 6,6'-p-Phenylen-di-<2-oxo-4-phenyl-cyclohex-3-en-carbonsaeure-(1)-ethylester> (96772-34-8)

Guidance literature:

With sodium ethanolate; In ethanol; at 70 - 80 ℃; for 5h;

DOI:10.3109/14756366.2010.530263

Reference yield:

acetophenone (98-86-2) → 6,6'-p-Phenylen-di-<2-oxo-4-phenyl-cyclohex-3-en-carbonsaeure-(1)-ethylester> (96772-34-8)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydroxide / ethanol / 4 h / 0 °C

2: sodium ethanolate / ethanol / 5 h / 70 - 80 °C

With sodium ethanolate; sodium hydroxide; In ethanol; 1: Claisen-Schmidt condensation;

DOI:10.3109/14756366.2010.530263

Reference yield:

→ 6,6'-p-Phenylen-di-<2-oxo-4-phenyl-cyclohex-3-en-carbonsaeure-(1)-ethylester> (96772-34-8)

Guidance literature:

3,3'-p-Phenylen-di-<1-phenyl-prop-2-en-1-on>, Acetessigsaeure-ethylester, Na-Ethylat, sd. A.;

DOI:10.1039/jr9630004386

upstream raw materials:

1,4-bis-(3-oxo-3-phenyl-propenyl)-benzene

ethyl acetoacetate

acetophenone

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