2-(2-bromophenyl)-4H-3,1-benzoxazin-4-one

Base Information

Chemical Name:2-(2-bromophenyl)-4H-3,1-benzoxazin-4-one
CAS No.:18595-86-3
Molecular Formula:C₁₄H₈BrNO₂
Molecular Weight:302.127
Hs Code.:
DSSTox Substance ID:DTXSID901273108
ChEMBL ID:CHEMBL158541
Mol file:18595-86-3.mol

Synonyms:2-(2-bromophenyl)-4H-3,1-benzoxazin-4-one;18595-86-3;MLS001210119;CHEMBL158541;2-(2-Bromo-phenyl)-benzo[d][1,3]oxazin-4-one;SMR000504992;SR-01000486344;SCHEMBL5299192;DTXSID901273108;HMS2817C16;BDBM50289006;CCG-19904;STK300106;AKOS000540944;SR-01000486344-1;SR-01000486344-3

Suppliers and Price of 2-(2-bromophenyl)-4H-3,1-benzoxazin-4-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2-(2-BROMOPHENYL)-4H-3,1-BENZOXAZIN-4-ONE 95.00%
5MG
$ 499.24

Total 0 raw suppliers

Chemical Property of 2-(2-bromophenyl)-4H-3,1-benzoxazin-4-one

Chemical Property:

XLogP3:3.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:300.97384
Heavy Atom Count:18
Complexity:369

Purity/Quality:: 2-(2-BROMOPHENYL)-4H-3,1-BENZOXAZIN-4-ONE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C(=O)OC(=N2)C3=CC=CC=C3Br

Technology Process of 2-(2-bromophenyl)-4H-3,1-benzoxazin-4-one

There total 11 articles about 2-(2-bromophenyl)-4H-3,1-benzoxazin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 118-92-3,159201-01-1,50816-84-7,80206-34-4,104809-47-4
anthranilic acid

: 7154-66-7
2-bromobenzoic acid chloride

: 18595-86-3
2-(2-bromophenyl)-4H-benzo[d][1,3]oxazin-4-one

Guidance literature:: With pyridine; at 0 - 20 ℃;
DOI:10.14233/ajchem.2013.12846 DOI:10.14233/ajchem.2014.16108

Reference yield: 81.0%

: 201230-82-2
carbon monoxide

: 304690-59-3
(1H-benzo[d][1,2,3]triazol-1-yl)(2-bromophenyl)methanone

: 18595-86-3
2-(2-bromophenyl)-4H-benzo[d][1,3]oxazin-4-one

Guidance literature:: With silver trifluoromethanesulfonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; palladium dichloride; In acetonitrile; at 120 ℃; for 16h; under 15001.5 Torr; Inert atmosphere; Autoclave;
DOI:10.1021/acs.orglett.7b03184

Reference yield: 61.0%

: 1022-46-4
2-phenyl-4H-3,1-benzoxazin-4-one

: 18595-86-3
2-(2-bromophenyl)-4H-benzo[d][1,3]oxazin-4-one

Guidance literature:: With N-Bromosuccinimide; palladium diacetate; toluene-4-sulfonic acid; In 1,2-dichloro-ethane; at 100 ℃; for 4h;
DOI:10.1039/c7ob01534h