1-O-pivaloyl-2-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-3-O-allyl-sn-glycerol

Base Information

Chemical Name:1-O-pivaloyl-2-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-3-O-allyl-sn-glycerol
CAS No.:73485-57-1
Molecular Formula:C₄₅H₅₄O₉
Molecular Weight:738.918
Hs Code.:

Synonyms:1-O-pivaloyl-2-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-3-O-allyl-sn-glycerol

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Chemical Property of 1-O-pivaloyl-2-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-3-O-allyl-sn-glycerol

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Technology Process of 1-O-pivaloyl-2-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-3-O-allyl-sn-glycerol

There total 4 articles about 1-O-pivaloyl-2-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-3-O-allyl-sn-glycerol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 4196-35-4
2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl bromide

: 73485-55-9
1-O-pivaloyl-3-O-allyl-sn-glycerol

: 73485-57-1
1-O-pivaloyl-2-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-3-O-allyl-sn-glycerol

Guidance literature:: With N-ethyl-N,N-diisopropylamine; tetraethylammonium bromide; In dichloromethane; N,N-dimethyl-formamide; for 96h; Ambient temperature;
DOI:10.1016/S0040-4020(01)98907-0

Reference yield:

: 4196-36-5
2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl 4-nitrobenzoate

: 73485-57-1
1-O-pivaloyl-2-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-3-O-allyl-sn-glycerol

Guidance literature:: Multi-step reaction with 2 steps

1: HBr / CH₂Cl₂ / 0.17 h / Ambient temperature

2: 60 percent / di-isopropyl-ethylamine / tetraethylammonium bromide / CH₂Cl₂; dimethylformamide / 96 h / Ambient temperature

With hydrogen bromide; N-ethyl-N,N-diisopropylamine; tetraethylammonium bromide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)98907-0

Reference yield:

: 123-34-2,73485-54-8,90940-93-5,55941-86-1
(R)-3-allyloxypropane-1,2-diol

: 73485-57-1
1-O-pivaloyl-2-O-(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)-3-O-allyl-sn-glycerol

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / pyridine / 1 h / -10 °C

2: 60 percent / di-isopropyl-ethylamine / tetraethylammonium bromide / CH₂Cl₂; dimethylformamide / 96 h / Ambient temperature

With N-ethyl-N,N-diisopropylamine; tetraethylammonium bromide; In pyridine; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)98907-0