1,10-phenanthroline-2-carboxamide-phenyl-4-ethoxypiperidine palladium(II) chloride

Base Information

Chemical Name:1,10-phenanthroline-2-carboxamide-phenyl-4-ethoxypiperidine palladium(II) chloride
CAS No.:956111-26-5
Molecular Formula:C₂₆H₂₅ClN₄O₂Pd
Molecular Weight:567.383
Hs Code.:

Synonyms:1,10-phenanthroline-2-carboxamide-phenyl-4-ethoxypiperidine palladium(II) chloride

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Chemical Property of 1,10-phenanthroline-2-carboxamide-phenyl-4-ethoxypiperidine palladium(II) chloride

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Technology Process of 1,10-phenanthroline-2-carboxamide-phenyl-4-ethoxypiperidine palladium(II) chloride

There total 4 articles about 1,10-phenanthroline-2-carboxamide-phenyl-4-ethoxypiperidine palladium(II) chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 12107-56-1
dichloro(cycloocta-1,5-diene)palladium (II)

: 956111-36-7
1,10-phenanthroline-2-carboxamide-phenyl-4-ethoxypiperidine

: 956111-26-5
1,10-phenanthroline-2-carboxamide-phenyl-4-ethoxypiperidine palladium(II) chloride

Guidance literature:: With tetrabutylammonium acetate; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: 956111-34-5
4-hydroxyphenyl-1,10-phenanthroline-2-carboxamide

: 956111-26-5
1,10-phenanthroline-2-carboxamide-phenyl-4-ethoxypiperidine palladium(II) chloride

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / N,N-dimethyl-formamide

2: N,N-dimethyl-formamide / 74 h / 20 - 110 °C

3: tetrabutylammonium acetate / N,N-dimethyl-formamide / 20 °C

With tetrabutylammonium acetate; sodium hydride; In N,N-dimethyl-formamide;

Reference yield:

: 36309-42-9
4-(trimethylsilyloxy)aniline

: 956111-26-5
1,10-phenanthroline-2-carboxamide-phenyl-4-ethoxypiperidine palladium(II) chloride

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / dichloromethane / 12 h / Heating / reflux

2: sodium hydride / N,N-dimethyl-formamide

3: N,N-dimethyl-formamide / 74 h / 20 - 110 °C

4: tetrabutylammonium acetate / N,N-dimethyl-formamide / 20 °C

With tetrabutylammonium acetate; sodium hydride; triethylamine; In dichloromethane; N,N-dimethyl-formamide;