{5-(4-methoxybenzoyl)-3,4-bis(4-methoxyphenyl)-1-[2-(4-methoxyphenyl)ethyl]-1H-pyrrol-2-yl}-(4-methoxyphenyl)methanone

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Chemical Name:{5-(4-methoxybenzoyl)-3,4-bis(4-methoxyphenyl)-1-[2-(4-methoxyphenyl)ethyl]-1H-pyrrol-2-yl}-(4-methoxyphenyl)methanone
CAS No.:917479-33-5
Molecular Formula:C₄₃H₃₉NO₇
Molecular Weight:681.785
Hs Code.:

Synonyms:{5-(4-methoxybenzoyl)-3,4-bis(4-methoxyphenyl)-1-[2-(4-methoxyphenyl)ethyl]-1H-pyrrol-2-yl}-(4-methoxyphenyl)methanone

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Chemical Property of {5-(4-methoxybenzoyl)-3,4-bis(4-methoxyphenyl)-1-[2-(4-methoxyphenyl)ethyl]-1H-pyrrol-2-yl}-(4-methoxyphenyl)methanone

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Technology Process of {5-(4-methoxybenzoyl)-3,4-bis(4-methoxyphenyl)-1-[2-(4-methoxyphenyl)ethyl]-1H-pyrrol-2-yl}-(4-methoxyphenyl)methanone

There total 4 articles about {5-(4-methoxybenzoyl)-3,4-bis(4-methoxyphenyl)-1-[2-(4-methoxyphenyl)ethyl]-1H-pyrrol-2-yl}-(4-methoxyphenyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 104-92-7
1-bromo-4-methoxy-benzene

: 570402-59-4
3,4-bis(4-methoxyphenyl)-1-[2-(4-methoxyphenyl)ethyl]pyrrole-2,5-dicarboxylic acid dimethyl ester

: 917479-33-5
{5-(4-methoxybenzoyl)-3,4-bis(4-methoxyphenyl)-1-[2-(4-methoxyphenyl)ethyl]-1H-pyrrol-2-yl}-(4-methoxyphenyl)methanone

Guidance literature:: 1-bromo-4-methoxy-benzene; With magnesium; In tetrahydrofuran;

3,4-bis(4-methoxyphenyl)-1-[2-(4-methoxyphenyl)ethyl]pyrrole-2,5-dicarboxylic acid dimethyl ester; In tetrahydrofuran; at 20 ℃; for 18h; Further stages.;
DOI:10.1055/s-2006-950190

Reference yield:

: 917479-37-9
3,4-bis(4-methoxyphenyl)-1-[2-(4-methoxyphenyl)ethyl]pyrrole-2,5-dicarboxylic acid

: 917479-33-5
{5-(4-methoxybenzoyl)-3,4-bis(4-methoxyphenyl)-1-[2-(4-methoxyphenyl)ethyl]-1H-pyrrol-2-yl}-(4-methoxyphenyl)methanone

Guidance literature:: Multi-step reaction with 2 steps

1.1: 94 percent / DBU / dimethylformamide / 18 h / 20 °C

2.1: Mg / tetrahydrofuran

2.2: 66 percent / tetrahydrofuran / 18 h / 20 °C

With magnesium; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1055/s-2006-950190

Reference yield:

: 28030-16-2
3-(4-methoxyphenyl)-2-oxopropanoic acid

: 917479-33-5
{5-(4-methoxybenzoyl)-3,4-bis(4-methoxyphenyl)-1-[2-(4-methoxyphenyl)ethyl]-1H-pyrrol-2-yl}-(4-methoxyphenyl)methanone

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-BuLi / tetrahydrofuran; hexane / 0.33 h / -78 °C

1.2: 67 percent / I₂; 4 Angstroem molecular sieves / tetrahydrofuran; hexane / 19 h / 20 °C

2.1: 94 percent / DBU / dimethylformamide / 18 h / 20 °C

3.1: Mg / tetrahydrofuran

3.2: 66 percent / tetrahydrofuran / 18 h / 20 °C

With n-butyllithium; magnesium; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; hexane; N,N-dimethyl-formamide;
DOI:10.1055/s-2006-950190