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Technology Process of [Fe(O)((C5H2N(C6H2(CH3)3))3(C5H2N(C6H2(C(CH3)3)(O)(C(CH3)2)C6H2(C(CH3)3)CO2CH3)))]

[Fe(O)((C5H2N(C6H2(CH3)3))3(C5H2N(C6H2(C(CH3)3)(O)(C(CH3)2)C6H2(C(CH3)3)CO2CH3)))]

Base Information
  • Chemical Name:[Fe(O)((C5H2N(C6H2(CH3)3))3(C5H2N(C6H2(C(CH3)3)(O)(C(CH3)2)C6H2(C(CH3)3)CO2CH3)))]
  • CAS No.:331716-54-2
  • Molecular Formula:C72H72FeN4O4
  • Molecular Weight:1113.24
  • Hs Code.:
[Fe(O)((C<sub>5</sub>H<sub>2</sub>N(C<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)3))3(C<sub>5</sub>H<sub>2</sub>N(C<sub>6</sub>H<sub>2</sub>(C(CH<sub>3</sub>)3)(O)(C(CH<sub>3</sub>)2)C<sub>6</sub>H<sub>2</sub>(C(CH<sub>3</sub>)3)CO<sub>2</sub>CH<sub>3</sub>)))]

Synonyms:[Fe(O)((C5H2N(C6H2(CH3)3))3(C5H2N(C6H2(C(CH3)3)(O)(C(CH3)2)C6H2(C(CH3)3)CO2CH3)))]

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Chemical Property of [Fe(O)((C5H2N(C6H2(CH3)3))3(C5H2N(C6H2(C(CH3)3)(O)(C(CH3)2)C6H2(C(CH3)3)CO2CH3)))]
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Technology Process of [Fe(O)((C5H2N(C6H2(CH3)3))3(C5H2N(C6H2(C(CH3)3)(O)(C(CH3)2)C6H2(C(CH3)3)CO2CH3)))]

There total 3 articles about [Fe(O)((C5H2N(C6H2(CH3)3))3(C5H2N(C6H2(C(CH3)3)(O)(C(CH3)2)C6H2(C(CH3)3)CO2CH3)))] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[FeOH((C<sub>5</sub>H<sub>2</sub>N(C<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)3))3(C<sub>5</sub>H<sub>2</sub>N(C<sub>6</sub>H<sub>2</sub>(C(CH<sub>3</sub>)3)(O)(C(CH<sub>3</sub>)2)C<sub>6</sub>H<sub>2</sub>(C(CH<sub>3</sub>)3)CO<sub>2</sub>CH<sub>3</sub>)))]*C<sub>5</sub>H<sub>12</sub>*H<sub>2</sub>O

[FeOH((C5H2N(C6H2(CH3)3))3(C5H2N(C6H2(C(CH3)3)(O)(C(CH3)2)C6H2(C(CH3)3)CO2CH3)))]*C5H12*H2O

[Fe(O)((C<sub>5</sub>H<sub>2</sub>N(C<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)3))3(C<sub>5</sub>H<sub>2</sub>N(C<sub>6</sub>H<sub>2</sub>(C(CH<sub>3</sub>)3)(O)(C(CH<sub>3</sub>)2)C<sub>6</sub>H<sub>2</sub>(C(CH<sub>3</sub>)3)CO<sub>2</sub>CH<sub>3</sub>)))]
331716-54-2

[Fe(O)((C5H2N(C6H2(CH3)3))3(C5H2N(C6H2(C(CH3)3)(O)(C(CH3)2)C6H2(C(CH3)3)CO2CH3)))]

Guidance literature:
With 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; Fe complex was reacted with m-chloroperoxybenzoic acid in THF at -61°C; not isolated; UV monitoring;
DOI:10.1021/ja028548o

Reference yield:

C<sub>20</sub>H<sub>8</sub>N<sub>4</sub>(C<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)3)3((CH<sub>3</sub>)2C<sub>13</sub>H<sub>4</sub>O(C(CH<sub>3</sub>)3)2COOCH<sub>3</sub>)FeOH
331716-52-0

C20H8N4(C6H2(CH3)3)3((CH3)2C13H4O(C(CH3)3)2COOCH3)FeOH

peroxyphenylacetic acid
19910-09-9

peroxyphenylacetic acid

[Fe(O)((C<sub>5</sub>H<sub>2</sub>N(C<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)3))3(C<sub>5</sub>H<sub>2</sub>N(C<sub>6</sub>H<sub>2</sub>(C(CH<sub>3</sub>)3)(O)(C(CH<sub>3</sub>)2)C<sub>6</sub>H<sub>2</sub>(C(CH<sub>3</sub>)3)CO<sub>2</sub>CH<sub>3</sub>)))]
331716-54-2

[Fe(O)((C5H2N(C6H2(CH3)3))3(C5H2N(C6H2(C(CH3)3)(O)(C(CH3)2)C6H2(C(CH3)3)CO2CH3)))]

Guidance literature:
In toluene; -40 °C under inert atm.; not isolated, UV anal.;
DOI:10.1021/ja0683032

Reference yield:

C<sub>20</sub>H<sub>8</sub>N<sub>4</sub>(C<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)3)3((CH<sub>3</sub>)2C<sub>13</sub>H<sub>4</sub>O(C(CH<sub>3</sub>)3)2COOCH<sub>3</sub>)FeOH
331716-52-0

C20H8N4(C6H2(CH3)3)3((CH3)2C13H4O(C(CH3)3)2COOCH3)FeOH

3-chloro-benzenecarboperoxoic acid
937-14-4

3-chloro-benzenecarboperoxoic acid

[Fe(O)((C<sub>5</sub>H<sub>2</sub>N(C<sub>6</sub>H<sub>2</sub>(CH<sub>3</sub>)3))3(C<sub>5</sub>H<sub>2</sub>N(C<sub>6</sub>H<sub>2</sub>(C(CH<sub>3</sub>)3)(O)(C(CH<sub>3</sub>)2)C<sub>6</sub>H<sub>2</sub>(C(CH<sub>3</sub>)3)CO<sub>2</sub>CH<sub>3</sub>)))]
331716-54-2

[Fe(O)((C5H2N(C6H2(CH3)3))3(C5H2N(C6H2(C(CH3)3)(O)(C(CH3)2)C6H2(C(CH3)3)CO2CH3)))]

Guidance literature:
In toluene; -20 °C under inert atm.; not isolated, UV anal.; Kinetics;
DOI:10.1021/ja0683032
upstream raw materials:

C20H8N4(C6H2(CH3)3)3((CH3)2C13H4O(C(CH3)3)2COOCH3)FeOH

3-chloro-benzenecarboperoxoic acid

peroxyphenylacetic acid

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