1-[(2,2,3,3-tetrafluoropropyl)oxy]ethyl bis(4-chlorophenethyl)phosphinothioselenoate

Base Information

• Chemical Name: 1-[(2,2,3,3-tetrafluoropropyl)oxy]ethyl bis(4-chlorophenethyl)phosphinothioselenoate
• CAS No.: 1443532-82-8
• Molecular Formula: C₂₁H₂₃Cl₂F₄OPSSe
• Molecular Weight: 580.312
• Mol file: 1443532-82-8.mol

Synonyms:1-[(2,2,3,3-tetrafluoropropyl)oxy]ethyl bis(4-chlorophenethyl)phosphinothioselenoate

Chemical Property of 1-[(2,2,3,3-tetrafluoropropyl)oxy]ethyl bis(4-chlorophenethyl)phosphinothioselenoate

Chemical Property:

Purity/Quality:

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Technology Process of 1-[(2,2,3,3-tetrafluoropropyl)oxy]ethyl bis(4-chlorophenethyl)phosphinothioselenoate

There total 1 articles about 1-[(2,2,3,3-tetrafluoropropyl)oxy]ethyl bis(4-chlorophenethyl)phosphinothioselenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bis(4-chlorophenethyl)phosphine sulfide (1428677-26-2) + 2,2,3,3-tetrafluoro-propan-1-ol vinyl ether (29819-80-5) → 1-[(2,2,3,3-tetrafluoropropyl)oxy]ethyl bis(4-chlorophenethyl)phosphinothioselenoate (1443532-82-8) + 1-[(2,2,3,3-tetrafluoropropyl)oxy]ethyl bis(4-chlorophenethyl)phosphinoselenothioate (1443532-83-9)

Guidance literature:

With selenium; In 1,4-dioxane; at 100 ℃; for 0.666667h; Overall yield = 81 %; Overall yield = 470 mg; Mechanism; Inert atmosphere;

DOI:10.1016/j.tet.2013.05.038

upstream raw materials:

bis(4-chlorophenethyl)phosphine sulfide

2,2,3,3-tetrafluoro-propan-1-ol vinyl ether