N²-benzoyl-5-methyl-1-(2,3,4-tri-O-benzoyl-β-D-ribopyranosyl)isocytosine

Base Information

Chemical Name:N²-benzoyl-5-methyl-1-(2,3,4-tri-O-benzoyl-β-D-ribopyranosyl)isocytosine
CAS No.:884592-98-7
Molecular Formula:C₃₈H₃₁N₃O₉
Molecular Weight:673.679
Hs Code.:

N<sup>2</sup>-benzoyl-5-methyl-1-(2,3,4-tri-O-benzoyl-β-D-ribopyranosyl)isocytosine

Synonyms:N²-benzoyl-5-methyl-1-(2,3,4-tri-O-benzoyl-β-D-ribopyranosyl)isocytosine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N²-benzoyl-5-methyl-1-(2,3,4-tri-O-benzoyl-β-D-ribopyranosyl)isocytosine

Chemical Property:

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Technology Process of N²-benzoyl-5-methyl-1-(2,3,4-tri-O-benzoyl-β-D-ribopyranosyl)isocytosine

There total 2 articles about N²-benzoyl-5-methyl-1-(2,3,4-tri-O-benzoyl-β-D-ribopyranosyl)isocytosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 884592-97-6
N²-benzoyl-5-methylisocytosine

: 10416-59-8
N,O-bis-(trimethylsilyl)-acetamide

: 1,2,3,4-tetra-O-benzoyl-D-ribopyranose

: 884592-98-7
N²-benzoyl-5-methyl-1-(2,3,4-tri-O-benzoyl-β-D-ribopyranosyl)isocytosine

Guidance literature:: N²-benzoyl-5-methylisocytosine; N,O-bis-(trimethylsilyl)-acetamide; 1,2,3,4-tetra-O-benzoyl-D-ribopyranose; In acetonitrile; at 60 ℃; for 0.5h;

With trimethylsilyl trifluoromethanesulfonate; In acetonitrile; at 60 ℃; for 2h;
DOI:10.1002/hlca.200690024

Reference yield:

: 98-88-4
benzoyl chloride

: 884592-98-7
N²-benzoyl-5-methyl-1-(2,3,4-tri-O-benzoyl-β-D-ribopyranosyl)isocytosine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 90 percent / pyridine / 20 h / 20 °C

2.1: acetonitrile / 0.5 h / 60 °C

2.2: trimethylsilyl trifluoromethanesulfonate / acetonitrile / 2 h / 60 °C

With pyridine; In acetonitrile;
DOI:10.1002/hlca.200690024