10-(4-carboxyphenyl)-5,5-bis(3-(2-methoxyethoxy)prop-1-yn-1-yl)-1,3,7,9-tetramethyl-5H-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinin-4-ium-5-uide

Base Information

Chemical Name:10-(4-carboxyphenyl)-5,5-bis(3-(2-methoxyethoxy)prop-1-yn-1-yl)-1,3,7,9-tetramethyl-5H-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinin-4-ium-5-uide
CAS No.:1232501-49-3
Molecular Formula:C₃₂H₃₇BN₂O₆
Molecular Weight:556.467
Hs Code.:

Synonyms:10-(4-carboxyphenyl)-5,5-bis(3-(2-methoxyethoxy)prop-1-yn-1-yl)-1,3,7,9-tetramethyl-5H-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinin-4-ium-5-uide

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Chemical Property of 10-(4-carboxyphenyl)-5,5-bis(3-(2-methoxyethoxy)prop-1-yn-1-yl)-1,3,7,9-tetramethyl-5H-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinin-4-ium-5-uide

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Technology Process of 10-(4-carboxyphenyl)-5,5-bis(3-(2-methoxyethoxy)prop-1-yn-1-yl)-1,3,7,9-tetramethyl-5H-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinin-4-ium-5-uide

There total 4 articles about 10-(4-carboxyphenyl)-5,5-bis(3-(2-methoxyethoxy)prop-1-yn-1-yl)-1,3,7,9-tetramethyl-5H-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinin-4-ium-5-uide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 201230-82-2
carbon monoxide

: 1221262-42-5
10-(4-iodophenyl)-5,5-bis(3-(2-methoxyethoxy)prop-1-yn-1-yl)-1,3,7,9-tetramethyl-5H-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinin-4-ium-5-uide

: 1232501-49-3
10-(4-carboxyphenyl)-5,5-bis(3-(2-methoxyethoxy)prop-1-yn-1-yl)-1,3,7,9-tetramethyl-5H-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinin-4-ium-5-uide

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; water; triethylamine; In tert-butyl alcohol; benzene; at 70 ℃; for 7h;

Reference yield:

: 1221262-42-5
10-(4-iodophenyl)-5,5-bis(3-(2-methoxyethoxy)prop-1-yn-1-yl)-1,3,7,9-tetramethyl-5H-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinin-4-ium-5-uide

: 1232501-49-3
10-(4-carboxyphenyl)-5,5-bis(3-(2-methoxyethoxy)prop-1-yn-1-yl)-1,3,7,9-tetramethyl-5H-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinin-4-ium-5-uide

Guidance literature:: Multi-step reaction with 2 steps

1: bis-triphenylphosphine-palladium(II) chloride; triethylamine / benzene / Heating

2: sodium hydroxide / ethanol; dichloromethane; water / 3 h / 20 °C

With bis-triphenylphosphine-palladium(II) chloride; triethylamine; sodium hydroxide; In ethanol; dichloromethane; water; benzene;
DOI:10.1021/jo300477p

Reference yield:

: 31995-08-1
3-(2-methoxyethoxy)prop-1-yne

: 1232501-49-3
10-(4-carboxyphenyl)-5,5-bis(3-(2-methoxyethoxy)prop-1-yn-1-yl)-1,3,7,9-tetramethyl-5H-dipyrrolo[1,2-c:2',1'-f][1,3,2]diazaborinin-4-ium-5-uide

Guidance literature:: Multi-step reaction with 3 steps

1.1: ethylmagnesium bromide / tetrahydrofuran / 2 h / 60 °C

1.2: 60 °C

2.1: bis-triphenylphosphine-palladium(II) chloride; triethylamine / benzene / Heating

3.1: sodium hydroxide / ethanol; dichloromethane; water / 3 h / 20 °C

With bis-triphenylphosphine-palladium(II) chloride; ethylmagnesium bromide; triethylamine; sodium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; water; benzene;
DOI:10.1021/jo300477p