C₂₁H₂₇N₃O₇

Base Information

Chemical Name:C₂₁H₂₇N₃O₇
CAS No.:1269428-60-5
Molecular Formula:C₂₁H₂₇N₃O₇
Molecular Weight:433.461
Hs Code.:

C<sub>21</sub>H<sub>27</sub>N<sub>3</sub>O<sub>7</sub>

Synonyms:C₂₁H₂₇N₃O₇

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Chemical Property of C₂₁H₂₇N₃O₇

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Technology Process of C₂₁H₂₇N₃O₇

There total 4 articles about C₂₁H₂₇N₃O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1269428-59-2
Boc-Orn(Cbz)-Oxz(Ser)-OMe

: 1269428-60-5
C₂₁H₂₇N₃O₇

Guidance literature:: Boc-Orn(Cbz)-Oxz(Ser)-OMe; With water; sodium hydroxide; In methanol; at 20 ℃; for 2h; Inert atmosphere;

With hydrogenchloride; In methanol; water; pH=Ca. 5; Inert atmosphere;
DOI:10.1016/j.tet.2010.11.100

Reference yield:

: 2480-93-5
Boc-Orn(Z)-OH

: 1269428-60-5
C₂₁H₂₇N₃O₇

Guidance literature:: Multi-step reaction with 4 steps

1.1: benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane; N,N-dimethyl-formamide / 18 h / 0 - 20 °C / Inert atmosphere

2.1: (bis-(2-methoxyethyl)amino)sulfur trufluoride / dichloromethane / 7 h / -20 - 20 °C / Inert atmosphere

3.1: Bromotrichloromethane; 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere

4.1: water; sodium hydroxide / methanol / 2 h / 20 °C / Inert atmosphere

4.2: pH Ca_. 5 / Inert atmosphere

With Bromotrichloromethane; water; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; sodium hydroxide; (bis-(2-methoxyethyl)amino)sulfur trufluoride; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2010.11.100

Reference yield:

: 1269428-85-4
Boc-Orn(Cbz)-Ser-OMe

: 1269428-60-5
C₂₁H₂₇N₃O₇

Guidance literature:: Multi-step reaction with 3 steps

1.1: (bis-(2-methoxyethyl)amino)sulfur trufluoride / dichloromethane / 7 h / -20 - 20 °C / Inert atmosphere

2.1: Bromotrichloromethane; 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere

3.1: water; sodium hydroxide / methanol / 2 h / 20 °C / Inert atmosphere

3.2: pH Ca_. 5 / Inert atmosphere

With Bromotrichloromethane; water; 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium hydroxide; (bis-(2-methoxyethyl)amino)sulfur trufluoride; In methanol; dichloromethane;
DOI:10.1016/j.tet.2010.11.100