C₂₄H₃₁N₅O₃

Base Information

Chemical Name:C₂₄H₃₁N₅O₃
CAS No.:1246521-46-9
Molecular Formula:C₂₄H₃₁N₅O₃
Molecular Weight:437.542
Hs Code.:

C<sub>24</sub>H<sub>31</sub>N<sub>5</sub>O<sub>3</sub>

Synonyms:C₂₄H₃₁N₅O₃

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Chemical Property of C₂₄H₃₁N₅O₃

Chemical Property:

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Technology Process of C₂₄H₃₁N₅O₃

There total 7 articles about C₂₄H₃₁N₅O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1246521-02-7
C₁₀H₁₁N₃O₂

: 174799-52-1
tert-butyl {2-[benzylamino]ethyl}carbamate

: 1246521-46-9
C₂₄H₃₁N₅O₃

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 72h;

Reference yield:

: 36404-88-3
2-chloro-3-carbaldehydepyridine

: 1246521-46-9
C₂₄H₃₁N₅O₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: toluene-4-sulfonic acid; hydrazine hydrate / 21 h / 120 °C / Cooling with ice

2.1: potassium hydroxide; iodine / N,N-dimethyl-formamide / 1 h / 20 °C / Cooling with ice

3.1: sodium hydride / N,N-dimethyl-formamide / 3 h / Cooling with ice

3.2: 1 h / 20 °C / Cooling with ice

4.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / tetrahydrofuran / 16 h / Reflux; Inert atmosphere

5.1: trifluoroacetic acid / 2 h / Reflux

6.1: sodium hydroxide; water / ethanol / 3 h / 20 °C / Cooling with ice

6.2: pH 3 - 4 / Cooling with ice

7.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 72 h / 20 °C

With water; iodine; sodium hydride; benzotriazol-1-ol; toluene-4-sulfonic acid; hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; potassium hydroxide; sodium hydroxide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;

Reference yield:

: 117007-52-0
3-iodo-1H-pyrazolo[3,4-b]pyridine

: 1246521-46-9
C₂₄H₃₁N₅O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 3 h / Cooling with ice

1.2: 1 h / 20 °C / Cooling with ice

2.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / tetrahydrofuran / 16 h / Reflux; Inert atmosphere

3.1: trifluoroacetic acid / 2 h / Reflux

4.1: sodium hydroxide; water / ethanol / 3 h / 20 °C / Cooling with ice

4.2: pH 3 - 4 / Cooling with ice

5.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 72 h / 20 °C

With water; sodium hydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; sodium hydroxide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;