methyl-[O²,O³,O⁴-tribenzoyl-O⁶-(toluene-4-sulfonyl)-α-D-glucopyranoside]

Base Information

• Chemical Name: methyl-[O²,O³,O⁴-tribenzoyl-O⁶-(toluene-4-sulfonyl)-α-D-glucopyranoside]
• CAS No.: 1153940-62-5
• Molecular Formula: C₃₅H₃₂O₁₁S
• Molecular Weight: 660.698
• Mol file: 1153940-62-5.mol

Synonyms:methyl-[O²,O³,O⁴-tribenzoyl-O⁶-(toluene-4-sulfonyl)-α-D-glucopyranoside]

Chemical Property of methyl-[O²,O³,O⁴-tribenzoyl-O⁶-(toluene-4-sulfonyl)-α-D-glucopyranoside]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of methyl-[O²,O³,O⁴-tribenzoyl-O⁶-(toluene-4-sulfonyl)-α-D-glucopyranoside]

There total 5 articles about methyl-[O²,O³,O⁴-tribenzoyl-O⁶-(toluene-4-sulfonyl)-α-D-glucopyranoside] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzoyl chloride (98-88-4) + methyl 6-O-tosyl-α-D-glucopyranoside (6619-09-6) → methyl-[O2,O3,O4-tribenzoyl-O6-(toluene-4-sulfonyl)-α-D-glucopyranoside] (1153940-62-5)

Guidance literature:

With pyridine; at 20 ℃; for 1h;

DOI:10.1016/j.bmcl.2017.03.029

Reference yield:

methyl 2,3,4-tri-O-benzoylglucopyranoside (34234-44-1) + p-toluenesulfonyl chloride (98-59-9) → methyl-[O2,O3,O4-tribenzoyl-O6-(toluene-4-sulfonyl)-α-D-glucopyranoside] (1153940-62-5)

Guidance literature:

With pyridine;

Reference yield:

benzoyl chloride (98-88-4) → methyl-[O2,O3,O4-tribenzoyl-O6-(toluene-4-sulfonyl)-α-D-glucopyranoside] (1153940-62-5)

Guidance literature:

Multi-step reaction with 3 steps

1: pyridine

2: chloroform; hydrogen chloride

3: pyridine

With pyridine; hydrogenchloride; chloroform;

upstream raw materials:

methyl 2,3,4-tri-O-benzoylglucopyranoside

p-toluenesulfonyl chloride

benzoyl chloride

methyl 2,3,4-tri-O-benzoyl-6-O-triphenylmethyl-α-D-glucopyranoside

Downstream raw materials:

methyl 6-deoxy-6-iodo-2,3,4-tri-O-benzoyl-α-D-glucopyranoside

methyl 6-O-tosyl-α-D-glucopyranoside