N-[(6-Benzyloxycarbonylaminohexyl)(tert-butoxycarbonyl)-amino]phthalimide

Base Information

Chemical Name:N-[(6-Benzyloxycarbonylaminohexyl)(tert-butoxycarbonyl)-amino]phthalimide
CAS No.:1236324-41-6
Molecular Formula:C₂₇H₃₃N₃O₆
Molecular Weight:495.576
Hs Code.:

Synonyms:N-[(6-Benzyloxycarbonylaminohexyl)(tert-butoxycarbonyl)-amino]phthalimide

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Chemical Property of N-[(6-Benzyloxycarbonylaminohexyl)(tert-butoxycarbonyl)-amino]phthalimide

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Technology Process of N-[(6-Benzyloxycarbonylaminohexyl)(tert-butoxycarbonyl)-amino]phthalimide

There total 5 articles about N-[(6-Benzyloxycarbonylaminohexyl)(tert-butoxycarbonyl)-amino]phthalimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 34387-89-8
N-(tert-butoxycarbonylamino)phthalimide

: 17996-12-2
N-benzyloxycarbonyl-6-amino-1-hexanol

: 1236324-41-6
N-[(6-Benzyloxycarbonylaminohexyl)(tert-butoxycarbonyl)-amino]phthalimide

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

Reference yield:

: 4048-33-3
6-amino-1-hexanol

: 1236324-41-6
N-[(6-Benzyloxycarbonylaminohexyl)(tert-butoxycarbonyl)-amino]phthalimide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium carbonate / water; tetrahydrofuran / 2.75 h / 5 - 20 °C

2: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

With di-isopropyl azodicarboxylate; sodium carbonate; triphenylphosphine; In tetrahydrofuran; water; 2: Mitsunobu reaction;

Reference yield:

: 85-44-9
phthalic anhydride

: 1236324-41-6
N-[(6-Benzyloxycarbonylaminohexyl)(tert-butoxycarbonyl)-amino]phthalimide

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 2.5 h / Reflux

2: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; toluene; 2: Mitsunobu reaction;