2-hydroxy-N,N-bis(2-hydroxyethyl)ethaneammonium [(1-benzylindol-3-yl)sulfonyl]acetate

Base Information

Chemical Name:2-hydroxy-N,N-bis(2-hydroxyethyl)ethaneammonium [(1-benzylindol-3-yl)sulfonyl]acetate
CAS No.:1312670-97-5
Molecular Formula:C₆H₁₅NO₃*C₁₇H₁₅NO₄S
Molecular Weight:478.566
Hs Code.:

Synonyms:2-hydroxy-N,N-bis(2-hydroxyethyl)ethaneammonium [(1-benzylindol-3-yl)sulfonyl]acetate

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Chemical Property of 2-hydroxy-N,N-bis(2-hydroxyethyl)ethaneammonium [(1-benzylindol-3-yl)sulfonyl]acetate

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Technology Process of 2-hydroxy-N,N-bis(2-hydroxyethyl)ethaneammonium [(1-benzylindol-3-yl)sulfonyl]acetate

There total 7 articles about 2-hydroxy-N,N-bis(2-hydroxyethyl)ethaneammonium [(1-benzylindol-3-yl)sulfonyl]acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.7%

: 1237036-51-9
[(1-benzylindol-3-yl)sulfonyl]acetic acid

: 637-39-8,67924-33-8
triethanolamine hydrochloride

: 1312670-97-5
2-hydroxy-N,N-bis(2-hydroxyethyl)ethaneammonium [(1-benzylindol-3-yl)sulfonyl]acetate

Guidance literature:: [(1-benzylindol-3-yl)sulfonyl]acetic acid; for 1h; Reflux; Alkaline conditions;

triethanolamine hydrochloride; Reflux;
DOI:10.1134/S1070363218100353

Reference yield: 96.0%

: 102-71-6,64114-46-1
triethanolamine

: 1237036-51-9
[(1-benzylindol-3-yl)sulfonyl]acetic acid

: 1312670-97-5
2-hydroxy-N,N-bis(2-hydroxyethyl)ethaneammonium [(1-benzylindol-3-yl)sulfonyl]acetate

Guidance literature:: In ethanol; at 20 - 50 ℃;
DOI:10.1007/s11172-010-0384-9

Reference yield:

: 3377-71-7
N-benzylindole

: 1312670-97-5
2-hydroxy-N,N-bis(2-hydroxyethyl)ethaneammonium [(1-benzylindol-3-yl)sulfonyl]acetate

Guidance literature:: Multi-step reaction with 4 steps

1.1: iodine; potassium iodide / ethanol / 3 h / 30 - 40 °C / Inert atmosphere

2.1: hydrazine hydrate; sodium hydroxide / ethanol; water / 2 h / Heating; Inert atmosphere

2.2: 12 h / 5 °C / pH 1

3.1: dihydrogen peroxide; acetic anhydride / 24 h / 0 - 20 °C

4.1: ethanol / 20 - 50 °C

With hydrazine hydrate; dihydrogen peroxide; iodine; acetic anhydride; potassium iodide; sodium hydroxide; In ethanol; water;
DOI:10.1007/s11172-010-0384-9