5-methyl-2-(1H-pyrazol-1-yl)-1,3-benzendicarboxylic acid 1,3-dimethyl ester

Base Information

Chemical Name:5-methyl-2-(1H-pyrazol-1-yl)-1,3-benzendicarboxylic acid 1,3-dimethyl ester
CAS No.:1262659-74-4
Molecular Formula:C₁₄H₁₄N₂O₄
Molecular Weight:274.276
Hs Code.:

Synonyms:5-methyl-2-(1H-pyrazol-1-yl)-1,3-benzendicarboxylic acid 1,3-dimethyl ester

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Chemical Property of 5-methyl-2-(1H-pyrazol-1-yl)-1,3-benzendicarboxylic acid 1,3-dimethyl ester

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Technology Process of 5-methyl-2-(1H-pyrazol-1-yl)-1,3-benzendicarboxylic acid 1,3-dimethyl ester

There total 1 articles about 5-methyl-2-(1H-pyrazol-1-yl)-1,3-benzendicarboxylic acid 1,3-dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 20518-17-6
1-(4-methylphenyl)-1H-pyrazole

: 124-38-9,18923-20-1
carbon dioxide

: 6063-88-3
methoxydimethylaluminium

: 18107-18-1
diazomethyl-trimethyl-silane

: 84401-18-3
1-(2,4-dimethylphenyl)-(1H-pyrazole)

: 1262659-71-1
2-(1H-pyrazol-1-yl)-1,3-benzendicarboxylic acid 1,3-dimethyl ester

: 1262659-74-4
5-methyl-2-(1H-pyrazol-1-yl)-1,3-benzendicarboxylic acid 1,3-dimethyl ester

Guidance literature:: 1-(4-methylphenyl)-1H-pyrazole; carbon dioxide; methoxydimethylaluminium; With chlorobis(cyclooctene)rhodium(I) dimer; tricyclohexylphosphine; In methanol; N,N-dimethyl acetamide; at 70 ℃; for 8h; under 760.051 Torr; Inert atmosphere;

diazomethyl-trimethyl-silane; In methanol; diethyl ether; at 0 ℃; for 1h; regioselective reaction; Inert atmosphere;
DOI:10.1021/ja109097z