methyl 2-biphenyl-4-yl)methyl>amino>pyridine-3-carboxylate

Base Information

Chemical Name:methyl 2-biphenyl-4-yl)methyl>amino>pyridine-3-carboxylate
CAS No.:150869-58-2
Molecular Formula:C₂₄H₂₄N₆O₂
Molecular Weight:428.494
Hs Code.:

methyl 2-<N-propyl-N-<(2'-<1H-tetrazol-5-yl>biphenyl-4-yl)methyl>amino>pyridine-3-carboxylate

Synonyms:methyl 2-biphenyl-4-yl)methyl>amino>pyridine-3-carboxylate

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Chemical Property of methyl 2-biphenyl-4-yl)methyl>amino>pyridine-3-carboxylate

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Technology Process of methyl 2-biphenyl-4-yl)methyl>amino>pyridine-3-carboxylate

There total 16 articles about methyl 2-biphenyl-4-yl)methyl>amino>pyridine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 150869-57-1
methyl 2-amino>pyridine-3-carboxylate

: 150869-58-2
methyl 2-biphenyl-4-yl)methyl>amino>pyridine-3-carboxylate

Guidance literature:: With sodium azide; trimethyltin(IV)chloride; In toluene; for 70h; Heating;
DOI:10.1080/00397919308009863

Reference yield: 71.0%

: 2273-45-2
dimethyltin oxide

: 150869-57-1
methyl 2-amino>pyridine-3-carboxylate

: 150869-58-2
methyl 2-biphenyl-4-yl)methyl>amino>pyridine-3-carboxylate

Guidance literature:: With trimethylsilylazide; In toluene;

Reference yield:

: 49609-84-9
2-Chloronicotinoyl chloride

: 150869-58-2
2-{Propyl-[2'-(2H-tetrazol-5-yl)-biphenyl-4-ylmethyl]-amino}-nicotinic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 0.33 h / Heating

2: ethanol / 6 h / 100 °C

3: 1.) 1,3-dimethyl-3,4,5,6-tetrahydro-2-pyrimidinone, LiN(TMS)2 / 1.) THF, 0 deg C, 10 min, 2.) THF, RT, 90 min

4: 88percent aq. HCOOH / 2 h / Ambient temperature

With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; formic acid; lithium hexamethyldisilazane; In ethanol;
DOI:10.1021/jm00070a012