Technology Process of 2,6-di-(3-methylphenyl)pyridine
There total 4 articles about 2,6-di-(3-methylphenyl)pyridine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
2,6-Dibromopyridine;
With
3,3’-(pyridine-2,6-diylbis(1H-imidazole-3-ium-1,3-diyl))bis(propane-1-sulfonate); palladium diacetate; potassium carbonate;
In
water; acetonitrile;
at 20 ℃;
for 0.166667h;
Inert atmosphere;
Schlenk technique;
m-tolylboronic acid;
In
water; acetonitrile;
at 80 ℃;
for 12h;
Inert atmosphere;
Schlenk technique;
DOI:10.1039/c5ra10561g
- Guidance literature:
-
With
[2,2]bipyridinyl; tris-(dibenzylideneacetone)dipalladium(0); 2,2,2-trifluoroacetic acid ammonia; trifluoroacetic acid;
In
methanol;
at 90 ℃;
for 48h;
Schlenk technique;
DOI:10.1021/acs.joc.9b02999
- Guidance literature:
-
With
iron(III) chloride; palladium diacetate; copper(II) acetate monohydrate; DavePhos;
In
dimethyl sulfoxide; N,N-dimethyl-formamide;
at 120 ℃;
for 40h;
Inert atmosphere;
DOI:10.1021/acs.joc.8b02971
