(S)-(-)-1-[1-(benzyloxymethyl)-2-(3,4-dimethoxyphenyl)ethyl]pyrrolidine-2,5-dione

Base Information

Chemical Name:(S)-(-)-1-[1-(benzyloxymethyl)-2-(3,4-dimethoxyphenyl)ethyl]pyrrolidine-2,5-dione
CAS No.:872516-12-6
Molecular Formula:C₂₂H₂₅NO₅
Molecular Weight:383.444
Hs Code.:

Synonyms:(S)-(-)-1-[1-(benzyloxymethyl)-2-(3,4-dimethoxyphenyl)ethyl]pyrrolidine-2,5-dione

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Chemical Property of (S)-(-)-1-[1-(benzyloxymethyl)-2-(3,4-dimethoxyphenyl)ethyl]pyrrolidine-2,5-dione

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Technology Process of (S)-(-)-1-[1-(benzyloxymethyl)-2-(3,4-dimethoxyphenyl)ethyl]pyrrolidine-2,5-dione

There total 5 articles about (S)-(-)-1-[1-(benzyloxymethyl)-2-(3,4-dimethoxyphenyl)ethyl]pyrrolidine-2,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: N-[1-benzyloxymethyl-2-(3,4-dimethoxy-phenyl)-ethyl]-succinamic acid

: 872516-12-6
(S)-(-)-1-[1-(benzyloxymethyl)-2-(3,4-dimethoxyphenyl)ethyl]pyrrolidine-2,5-dione

Guidance literature:: With sodium acetate; acetic anhydride; at 85 ℃; for 1h;
DOI:10.1021/jo051584w

Reference yield:

: 872516-08-0
(S)-(-)-1-(benzyloxymethyl)-2-(3,4-dimethoxyphenyl)ethylamine

: 872516-12-6
(S)-(-)-1-[1-(benzyloxymethyl)-2-(3,4-dimethoxyphenyl)ethyl]pyrrolidine-2,5-dione

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether / 16 h / Heating

2: 280 mg / NaOAc; Ac₂O / 1 h / 85 °C

With sodium acetate; acetic anhydride; In diethyl ether;
DOI:10.1021/jo051584w

Reference yield:

: 872516-04-6
(S)-(-)-[1-(benzyloxymethyl)-2-(3,4-dimethoxyphenyl)ethyl]carbamic acid tert-butyl ester

: 872516-12-6
(S)-(-)-1-[1-(benzyloxymethyl)-2-(3,4-dimethoxyphenyl)ethyl]pyrrolidine-2,5-dione

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / CF₃CO₂H / CH₂Cl₂ / 1 h / 20 °C

2: diethyl ether / 16 h / Heating

3: 280 mg / NaOAc; Ac₂O / 1 h / 85 °C

With sodium acetate; acetic anhydride; trifluoroacetic acid; In diethyl ether; dichloromethane;
DOI:10.1021/jo051584w