(R,Z)-N-(1-(benzyloxy)-3,3-dimethylbutan-2-yl)-1-(4-bromophenyl)methanimine oxide

Base Information

Chemical Name:(R,Z)-N-(1-(benzyloxy)-3,3-dimethylbutan-2-yl)-1-(4-bromophenyl)methanimine oxide
CAS No.:1612163-84-4
Molecular Formula:C₂₀H₂₄BrNO₂
Molecular Weight:390.32
Hs Code.:

Synonyms:(R,Z)-N-(1-(benzyloxy)-3,3-dimethylbutan-2-yl)-1-(4-bromophenyl)methanimine oxide

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Chemical Property of (R,Z)-N-(1-(benzyloxy)-3,3-dimethylbutan-2-yl)-1-(4-bromophenyl)methanimine oxide

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Technology Process of (R,Z)-N-(1-(benzyloxy)-3,3-dimethylbutan-2-yl)-1-(4-bromophenyl)methanimine oxide

There total 3 articles about (R,Z)-N-(1-(benzyloxy)-3,3-dimethylbutan-2-yl)-1-(4-bromophenyl)methanimine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1612163-82-2
(R)-N-(1-(benzyloxy)-3,3-dimethylbutan-2-yl)hydroxylamine

: 1122-91-4
4-bromo-benzaldehyde

: 1612163-84-4
(R,Z)-N-(1-(benzyloxy)-3,3-dimethylbutan-2-yl)-1-(4-bromophenyl)methanimine oxide

Guidance literature:: With magnesium sulfate; In dichloromethane; at 20 ℃; for 18h;
DOI:10.1021/jo500848a

Reference yield:

: 393536-67-9
(R)-1-(benzyloxymethyl)-2,2-dimethylpropylamine

: 1612163-84-4
(R,Z)-N-(1-(benzyloxy)-3,3-dimethylbutan-2-yl)-1-(4-bromophenyl)methanimine oxide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium carbonate; sodium hydroxide / dichloromethane; water / 18 h / 20 °C

2: ammonium hydroxide / methanol / 18 h / 20 °C

3: magnesium sulfate / dichloromethane / 18 h / 20 °C

With ammonium hydroxide; sodium carbonate; magnesium sulfate; sodium hydroxide; In methanol; dichloromethane; water;
DOI:10.1021/jo500848a

Reference yield:

: 1612163-80-0
(R)-O-benzoyl-N-(1-(benzyloxy)-3,3-dimethylbutan-2-yl)-hydroxylamine

: 1612163-84-4
(R,Z)-N-(1-(benzyloxy)-3,3-dimethylbutan-2-yl)-1-(4-bromophenyl)methanimine oxide

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium hydroxide / methanol / 18 h / 20 °C

2: magnesium sulfate / dichloromethane / 18 h / 20 °C

With ammonium hydroxide; magnesium sulfate; In methanol; dichloromethane;
DOI:10.1021/jo500848a