2-nitro-5-thiomorpholinophenol

Base Information

• Chemical Name: 2-nitro-5-thiomorpholinophenol
• CAS No.: 219689-84-6
• Molecular Formula: C₁₀H₁₂N₂O₃S
• Molecular Weight: 240.283

Synonyms:2-nitro-5-thiomorpholinophenol

Chemical Property of 2-nitro-5-thiomorpholinophenol

Chemical Property:

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Technology Process of 2-nitro-5-thiomorpholinophenol

There total 1 articles about 2-nitro-5-thiomorpholinophenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.1%

Thiomorpholin (123-90-0) + 5-fluoro-2-nitrophenol (446-36-6) → 2-nitro-5-thiomorpholinophenol (219689-84-6)

Guidance literature:

With 4-methyl-morpholine; In acetonitrile; at 80 ℃; for 3h;

DOI:10.1021/acs.jmedchem.0c00500

Reference yield:

2-nitro-5-thiomorpholinophenol (219689-84-6) → C10H14N2OS

Guidance literature:

With acetic acid; zinc; In tetrahydrofuran; at 30 - 40 ℃; Inert atmosphere;

DOI:10.1021/acs.jmedchem.0c00500

upstream raw materials:

Thiomorpholin

5-fluoro-2-nitrophenol

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