N^α-palmitoyl-N^ε-10,12-pentacosadiynoyl-(S)-lysinyl-(S)-alanyl-(S)-leucinyl-(S)-phenylalanyl-glycine

Base Information

• Chemical Name: N^α-palmitoyl-N^ε-10,12-pentacosadiynoyl-(S)-lysinyl-(S)-alanyl-(S)-leucinyl-(S)-phenylalanyl-glycine
• CAS No.: 284670-61-7
• Molecular Formula: C₆₇H₁₁₂N₆O₈
• Molecular Weight: 1129.66

Synonyms:N^α-palmitoyl-N^ε-10,12-pentacosadiynoyl-(S)-lysinyl-(S)-alanyl-(S)-leucinyl-(S)-phenylalanyl-glycine

Chemical Property of N^α-palmitoyl-N^ε-10,12-pentacosadiynoyl-(S)-lysinyl-(S)-alanyl-(S)-leucinyl-(S)-phenylalanyl-glycine

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Technology Process of N^α-palmitoyl-N^ε-10,12-pentacosadiynoyl-(S)-lysinyl-(S)-alanyl-(S)-leucinyl-(S)-phenylalanyl-glycine

There total 1 articles about N^α-palmitoyl-N^ε-10,12-pentacosadiynoyl-(S)-lysinyl-(S)-alanyl-(S)-leucinyl-(S)-phenylalanyl-glycine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

N-(fluoren-9-ylmethoxycarbonyl)glycine (29022-11-5) + Fmoc-Leu-OH (35661-60-0) + N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine (35661-39-3,136132-75-7) + N-Fmoc L-Phe (35661-40-6) → Nα-palmitoyl-Nε-10,12-pentacosadiynoyl-(S)-lysinyl-(S)-alanyl-(S)-leucinyl-(S)-phenylalanyl-glycine (284670-61-7)

Guidance literature:

N-(fluoren-9-ylmethoxycarbonyl)glycine; Fmoc-Leu-OH; N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine; N-Fmoc L-Phe; N^α-Fmoc-N^ε-Dde-Lys-OH; palmitic acid pentacosadiynoic acid;

With trifluoroacetic acid; In dichloromethane; Further stages.;

DOI:10.1021/jo991685s

Reference yield: 53.0%

3-aminopropyl-β-D-galactopyranoside (201667-53-0) + Nα-palmitoyl-Nε-10,12-pentacosadiynoyl-(S)-lysinyl-(S)-alanyl-(S)-leucinyl-(S)-phenylalanyl-glycine (284670-61-7) → Nα-palmitoyl-Nε-10,12-pentacosadiynoyl-(S)-lysinyl-(S)-alanyl-(S)-leucinyl-(S)-phenylalanyl-glycine[3-(β-D-galactopyranosyloxy)propyl]amide (284670-60-6)

Guidance literature:

With bis-2-propyl carbonate; benzotriazol-1-ol; In dichloromethane; N,N-dimethyl-formamide; for 5h;

DOI:10.1021/jo991685s

upstream raw materials:

N-(fluoren-9-ylmethoxycarbonyl)glycine

Fmoc-Leu-OH

N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-alanine

N-Fmoc L-Phe

Downstream raw materials:

N^α-palmitoyl-N^ε-10,12-pentacosadiynoyl-(S)-lysinyl-(S)-alanyl-(S)-leucinyl-(S)-phenylalanyl-glycine[3-(β-D-galactopyranosyloxy)propyl]amide

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