H₃B(PPh₂(C₆H₄Cl))

Base Information

• Chemical Name: H₃B(PPh₂(C₆H₄Cl))
• CAS No.: 1257322-31-8
• Molecular Formula: C₁₈H₁₇BClP
• Molecular Weight: 310.571
• Mol file: 1257322-31-8.mol

Synonyms:H₃B(PPh₂(C₆H₄Cl))

Chemical Property of H₃B(PPh₂(C₆H₄Cl))

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of H₃B(PPh₂(C₆H₄Cl))

There total 1 articles about H₃B(PPh₂(C₆H₄Cl)) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

1-Chloro-4-iodobenzene (637-87-6) + diphenylphosphineborane (41593-58-2) → H3B(PPh2(C6H4Cl)) (1257322-31-8)

Guidance literature:

With [PdCl(((OC₆H₄C₆H₄O)PO)2C₆H(tBu)2)]; potassium carbonate; In acetonitrile; at 40 ℃; for 16h; Inert atmosphere;

DOI:10.1016/j.jorganchem.2010.08.026

Reference yield: 89.0%

H3B(PPh2(C6H4Cl)) (1257322-31-8) → (4-chlorophenyl)diphenylphosphane (734-60-1)

Guidance literature:

In tetrahydrofuran; methanol; for 96h; Inert atmosphere; Molecular sieve; Reflux;

DOI:10.1016/j.jorganchem.2010.08.026

upstream raw materials:

1-Chloro-4-iodobenzene

diphenylphosphineborane

Downstream raw materials:

(4-chlorophenyl)diphenylphosphane