Pt(CH₂COMe)(Ph)(cod)

Base Information

Chemical Name:Pt(CH₂COMe)(Ph)(cod)
CAS No.:478294-12-1
Molecular Formula:C₁₇H₂₂OPt
Molecular Weight:437.441
Hs Code.:

Synonyms:Pt(CH₂COMe)(Ph)(cod)

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Chemical Property of Pt(CH₂COMe)(Ph)(cod)

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Technology Process of Pt(CH₂COMe)(Ph)(cod)

There total 4 articles about Pt(CH₂COMe)(Ph)(cod) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 366-18-7
[2,2]bipyridinyl

: [(Pt(Ph)(1,5-cyclooctadiene))2(μ-OH)](BF4)

: 67-64-1
acetone

: 478294-12-1
Pt(CH₂COMe)(Ph)(cod)

: 899439-54-4
[Pt(Ph)(bpy)(cod)](BF₄)

Guidance literature:: In acetone; under inert atm. to suspn. Pt complex in acetone bpy was added and stirred for 20 min at room temp.; hexane was added, ppt. was filtered - (Pt(Ph)(bpy)(cod))(BF4), filtrate was evapd. - Pt(CH2COMe)(Ph)(cod); elem. anal.;
DOI:10.1021/om060206u

Reference yield: 74.0%

: 51177-68-5
Pt(1,5-cyclooctadiene)(Ph)(I)

: 67-64-1
acetone

: diphenyl(1,5-cyclooctadiene)platinum(II)

: 478294-13-2
Pt(C₈H₁₂)(CH₂COCH₃)2

: 478294-12-1
Pt(CH₂COMe)(Ph)(cod)

Guidance literature:: With Ag₂O₃; In acetone; byproducts: AgI; heating in NMR tube to 50°C with acetone in the presence of Ag2O for 20 h; not isolated; monitored by NMR;
DOI:10.1021/om0204991

Reference yield: 66.0%

: 51177-68-5
Pt(1,5-cyclooctadiene)(Ph)(I)

: 67-64-1
acetone

: 478294-12-1
Pt(CH₂COMe)(Ph)(cod)

Guidance literature:: With Bu₄NOH; In methanol; diethyl ether; acetone; under inert atm. to soln. PtI(Ph)(cod) in Et2O-acetone Bu4NOH in MeOH was added and stirred for 1 h at room temp.; soln. was filtered and evapd., residue was dissolved in Et2O, washed with water, dried over MgSO4, filtered and evapd. in vacuo;
DOI:10.1021/om060206u