Technology Process of 1,4-dimethoxy-2,3-dimethyl-5-oxiranylbenzene
There total 3 articles about 1,4-dimethoxy-2,3-dimethyl-5-oxiranylbenzene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride;
In
tetrahydrofuran;
for 5h;
Ambient temperature;
DOI:10.1016/S0040-4020(01)91854-X
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 86 percent / HBr / acetic acid / 20.5 h / Ambient temperature
2: 92 percent / dimethyl selenoxide, dipotassium hydrogen phosphate / 1,2-dichloro-ethane / 8 h / Heating
3: 75 percent / NaOH, TEBA / tetrahydrofuran / 5 h / Ambient temperature
With
sodium hydroxide; dipotassium hydrogenphosphate; N-benzyl-N,N,N-triethylammonium chloride; hydrogen bromide; dimethyl selenoxide;
In
tetrahydrofuran; acetic acid; 1,2-dichloro-ethane;
DOI:10.1016/S0040-4020(01)91854-X
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 92 percent / dimethyl selenoxide, dipotassium hydrogen phosphate / 1,2-dichloro-ethane / 8 h / Heating
2: 75 percent / NaOH, TEBA / tetrahydrofuran / 5 h / Ambient temperature
With
sodium hydroxide; dipotassium hydrogenphosphate; N-benzyl-N,N,N-triethylammonium chloride; dimethyl selenoxide;
In
tetrahydrofuran; 1,2-dichloro-ethane;
DOI:10.1016/S0040-4020(01)91854-X
