4-phenyl chloroformate

Base Information

Chemical Name:4-phenyl chloroformate
CAS No.:219591-83-0
Molecular Formula:C₁₁H₁₂ClF₂NO₂
Molecular Weight:263.672
Hs Code.:

4-<bis(2-fluoroethyl)amino>phenyl chloroformate

Synonyms:4-phenyl chloroformate

Suppliers and Price of 4-phenyl chloroformate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-phenyl chloroformate

Chemical Property:

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Technology Process of 4-phenyl chloroformate

There total 4 articles about 4-phenyl chloroformate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.5%

: 75-44-5
phosgene

: 219592-00-4
4-[bis-(2-fluoro-ethyl)-amino]-phenol

: 219591-83-0
4-phenyl chloroformate

Guidance literature:: With triethylamine; In dichloromethane;
DOI:10.1021/jm980425k

Reference yield:

: 101582-69-8
4--O-benzylphenol

: 219591-83-0
4-phenyl chloroformate

Guidance literature:: Multi-step reaction with 4 steps

1: Et₃N, 4-(dimethylamino)pyridine / CH₂Cl₂ / 1 h

2: KF, 18-crown-6 ether / acetonitrile / 48 h / 60 °C

3: 98 percent / trifluoroacetic acid / various solvent(s) / 72 h / Ambient temperature

4: 74.5 percent / Et₃N / CH₂Cl₂

With dmap; potassium fluoride; 18-crown-6 ether; triethylamine; trifluoroacetic acid; In dichloromethane; acetonitrile;
DOI:10.1021/jm980425k

Reference yield:

: 219591-96-5
4--O-benzylphenol

: 219591-83-0
4-phenyl chloroformate

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / trifluoroacetic acid / various solvent(s) / 72 h / Ambient temperature

2: 74.5 percent / Et₃N / CH₂Cl₂

With triethylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jm980425k