2-benzylidene-N-(3-cyano-4,5,6,7-tetrahydrobenzo[b]thiophen-2-yl)-N'-phenylmalonamide

Base Information

Chemical Name:2-benzylidene-N-(3-cyano-4,5,6,7-tetrahydrobenzo[b]thiophen-2-yl)-N'-phenylmalonamide
CAS No.:1322643-97-9
Molecular Formula:C₂₅H₂₁N₃O₂S
Molecular Weight:427.527
Hs Code.:

Synonyms:2-benzylidene-N-(3-cyano-4,5,6,7-tetrahydrobenzo[b]thiophen-2-yl)-N'-phenylmalonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-benzylidene-N-(3-cyano-4,5,6,7-tetrahydrobenzo[b]thiophen-2-yl)-N'-phenylmalonamide

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Technology Process of 2-benzylidene-N-(3-cyano-4,5,6,7-tetrahydrobenzo[b]thiophen-2-yl)-N'-phenylmalonamide

There total 3 articles about 2-benzylidene-N-(3-cyano-4,5,6,7-tetrahydrobenzo[b]thiophen-2-yl)-N'-phenylmalonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1322643-95-7
N-(3-cyano-4,5,6,7-tetrahydrobenzo[b]thiophen-2-yl)-N'-phenylmalonamide

: 100-52-7
benzaldehyde

: 1322643-97-9
2-benzylidene-N-(3-cyano-4,5,6,7-tetrahydrobenzo[b]thiophen-2-yl)-N'-phenylmalonamide

Guidance literature:: With piperidine; In 1,4-dioxane; for 5h; Reflux;
DOI:10.3390/molecules16086271

Reference yield:

: 62-53-3
aniline

: 1322643-97-9
2-benzylidene-N-(3-cyano-4,5,6,7-tetrahydrobenzo[b]thiophen-2-yl)-N'-phenylmalonamide

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / 5 h / Reflux

2: piperidine / 1,4-dioxane / 5 h / Reflux

With piperidine; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.3390/molecules16086271

Reference yield:

: 348621-54-5
N-(3-cyano-4,5,6,7-tetrahydrobenzo[b]thiophen-2-yl)malonamic acid ethyl ester

: 1322643-97-9
2-benzylidene-N-(3-cyano-4,5,6,7-tetrahydrobenzo[b]thiophen-2-yl)-N'-phenylmalonamide

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / 5 h / Reflux

2: piperidine / 1,4-dioxane / 5 h / Reflux

With piperidine; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.3390/molecules16086271