C₂₆H₄₅NOSn

Base Information

• Chemical Name: C₂₆H₄₅NOSn
• CAS No.: 1049011-85-9
• Molecular Formula: C₂₆H₄₅NOSn
• Molecular Weight: 506.359

Synonyms:C₂₆H₄₅NOSn

Chemical Property of C₂₆H₄₅NOSn

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Technology Process of C₂₆H₄₅NOSn

There total 1 articles about C₂₆H₄₅NOSn which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

N-(4-(tert-butyl)phenyl)methacrylamide (20330-51-2) + tributyltin chloride (1461-22-9) → C26H45NOSn (1049011-85-9)

Guidance literature:

N-(p-tert-butylphenyl)methacrylamide; With potassium tert-butylate; In tetrahydrofuran; at -78 ℃; for 1h;

With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

tributyltin chloride; In tetrahydrofuran; hexane; for 1h;

DOI:10.1002/chem.201403357

Reference yield: 98.0%

methyl 2-oxo-2-phenylacetate (15206-55-0) + C26H45NOSn (1049011-85-9) → C23H27NO4

Guidance literature:

methyl 2-oxo-2-phenylacetate; With indium(III) triflate; (S,S)-2,6-bis(4-phenyl-2-oxazolinyl)pyridine; In acetonitrile; at 20 ℃; Molecular sieve; Inert atmosphere;

C₂₆H₄₅NOSn; In acetonitrile; at 20 ℃; for 16h; enantioselective reaction; Molecular sieve; Inert atmosphere;

DOI:10.1039/c4ob01508h

Reference yield: 92.0%

1-methyl-1H-indole-2,3-dione (2058-74-4) + C26H45NOSn (1049011-85-9) → C23H26N2O3

Guidance literature:

1-methyl-1H-indole-2,3-dione; With indium(III) triflate; (S,S)-2,6-bis(4-phenyl-2-oxazolinyl)pyridine; In acetonitrile; at 20 ℃; for 0.5h; Molecular sieve; Inert atmosphere;

C₂₆H₄₅NOSn; In acetonitrile; at 20 ℃; for 17h; enantioselective reaction; Molecular sieve; Inert atmosphere;

DOI:10.1002/chem.201403357

upstream raw materials:

N-(4-(tert-butyl)phenyl)methacrylamide

tributyltin chloride

Downstream raw materials:

(S)-N-(4-tert-butylphenyl)-4-hydroxy-2-methylene-4-(naphthalen-1-yl)butanamide

(S)-N-(4-tert-butylphenyl)-4-hydroxy-2-methylene-4-phenylbutanamide

(S)-N-(4-tert-butylphenyl)-4-(3-chlorophenyl)-4-hydroxy-2-methylenebutanamide

(S)-N-(4-tert-butylphenyl)-4-hydroxy-4-(4-isopropylphenyl)-2-methylenebutanamide

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