pyridin-3-yl-methylene-bis(3-isopentanoyl-5-formyl-2,4,6-trihydroxybenzene)

Base Information

Chemical Name:pyridin-3-yl-methylene-bis(3-isopentanoyl-5-formyl-2,4,6-trihydroxybenzene)
CAS No.:1367716-15-1
Molecular Formula:C₃₀H₃₁NO₁₀
Molecular Weight:565.577
Hs Code.:

Synonyms:pyridin-3-yl-methylene-bis(3-isopentanoyl-5-formyl-2,4,6-trihydroxybenzene)

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Chemical Property of pyridin-3-yl-methylene-bis(3-isopentanoyl-5-formyl-2,4,6-trihydroxybenzene)

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Technology Process of pyridin-3-yl-methylene-bis(3-isopentanoyl-5-formyl-2,4,6-trihydroxybenzene)

There total 4 articles about pyridin-3-yl-methylene-bis(3-isopentanoyl-5-formyl-2,4,6-trihydroxybenzene) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 500-22-1
3-pyridinecarboxaldehyde

: 78423-49-1
formyl isovaleryl phloroglucinol

: 1367716-15-1
pyridin-3-yl-methylene-bis(3-isopentanoyl-5-formyl-2,4,6-trihydroxybenzene)

Guidance literature:: With methanesulfonic acid; at 80 ℃; for 0.5h;
DOI:10.1016/j.bmcl.2012.01.089

Reference yield:

: 108-73-6
3,5-dihydroxyphenol

: 1367716-15-1
pyridin-3-yl-methylene-bis(3-isopentanoyl-5-formyl-2,4,6-trihydroxybenzene)

Guidance literature:: Multi-step reaction with 3 steps

1: aluminum (III) chloride; nitrobenzene / 1.5 h

2: N,N-dimethyl-formamide; trichlorophosphate / ethyl acetate / 1 h

3: methanesulfonic acid / 0.5 h / 80 °C

With aluminum (III) chloride; methanesulfonic acid; nitrobenzene; N,N-dimethyl-formamide; trichlorophosphate; In ethyl acetate; 1: Friedel Crafts acylation;
DOI:10.1016/j.bmcl.2012.01.089

Reference yield:

: 108-12-3
isopentanoyl chloride

: 1367716-15-1
pyridin-3-yl-methylene-bis(3-isopentanoyl-5-formyl-2,4,6-trihydroxybenzene)

Guidance literature:: Multi-step reaction with 3 steps

1: aluminum (III) chloride; nitrobenzene / 1.5 h

2: N,N-dimethyl-formamide; trichlorophosphate / ethyl acetate / 1 h

3: methanesulfonic acid / 0.5 h / 80 °C

With aluminum (III) chloride; methanesulfonic acid; nitrobenzene; N,N-dimethyl-formamide; trichlorophosphate; In ethyl acetate; 1: Friedel Crafts acylation;
DOI:10.1016/j.bmcl.2012.01.089