C₄₂H₃₅NO₉

Base Information

Chemical Name:C₄₂H₃₅NO₉
CAS No.:1315504-15-4
Molecular Formula:C₄₂H₃₅NO₉
Molecular Weight:697.741
Hs Code.:

C<sub>42</sub>H<sub>35</sub>NO<sub>9</sub>

Synonyms:C₄₂H₃₅NO₉

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Chemical Property of C₄₂H₃₅NO₉

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Technology Process of C₄₂H₃₅NO₉

There total 17 articles about C₄₂H₃₅NO₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1315503-86-6
C₃₅H₂₉NO₉

: 100-39-0
benzyl bromide

: 1315504-15-4
C₄₂H₃₅NO₉

Guidance literature:: With potassium carbonate; In acetone; at 20 ℃; for 4h;
DOI:10.1021/ja205339p

Reference yield:

: C₂₂H₂₅NO₄Si

: 1315504-15-4
C₄₂H₃₅NO₉

Guidance literature:: Multi-step reaction with 9 steps

1.1: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 1 h / 20 °C

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 20 °C

3.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.67 h / -78 °C

3.2: 0.08 h / 0 °C

4.1: borane-THF; (S)-Corey-Bakshi-Shibata oxazaborolidine / tetrahydrofuran; toluene / 2.5 h / -20 °C

5.1: ammonium cerium (IV) nitrate / water; acetonitrile / 0 °C

6.1: silver(l) oxide / dichloromethane / 18 h / 20 °C / Molecular sieve

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.17 h / 0 °C

8.1: sodium ethanolate / ethanol / 18 h / 20 - 60 °C / Molecular sieve

9.1: potassium carbonate / acetone / 4 h / 20 °C

With ammonium cerium (IV) nitrate; borane-THF; tetrabutyl ammonium fluoride; sodium ethanolate; potassium carbonate; acetic acid; N-ethyl-N,N-diisopropylamine; silver(l) oxide; lithium hexamethyldisilazane; (S)-Corey-Bakshi-Shibata oxazaborolidine; In tetrahydrofuran; ethanol; dichloromethane; water; acetone; toluene; acetonitrile;
DOI:10.1021/ja205339p

Reference yield:

: 1315503-82-2
7-(benzyloxy)-4-(methoxymethoxy)-3-oxo-1,3-dihydroisobenzofuran-1-carbonitrile

: 1315504-15-4
C₄₂H₃₅NO₉

Guidance literature:: Multi-step reaction with 7 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.67 h / -78 °C

1.2: 0.08 h / 0 °C

2.1: borane-THF; (S)-Corey-Bakshi-Shibata oxazaborolidine / tetrahydrofuran; toluene / 2.5 h / -20 °C

3.1: ammonium cerium (IV) nitrate / water; acetonitrile / 0 °C

4.1: silver(l) oxide / dichloromethane / 18 h / 20 °C / Molecular sieve

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.17 h / 0 °C

6.1: sodium ethanolate / ethanol / 18 h / 20 - 60 °C / Molecular sieve

7.1: potassium carbonate / acetone / 4 h / 20 °C

With ammonium cerium (IV) nitrate; borane-THF; tetrabutyl ammonium fluoride; sodium ethanolate; potassium carbonate; silver(l) oxide; lithium hexamethyldisilazane; (S)-Corey-Bakshi-Shibata oxazaborolidine; In tetrahydrofuran; ethanol; dichloromethane; water; acetone; toluene; acetonitrile;
DOI:10.1021/ja205339p