Technology Process of C32H49N5O8Si2
There total 9 articles about C32H49N5O8Si2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium tetrahydroborate;
In
ethanol; ethyl acetate;
at 0 ℃;
for 1h;
DOI:10.1021/jm401224y
- Guidance literature:
-
C33H51N5O9Si2;
With
sodium periodate;
In
tetrahydrofuran; water;
at 20 ℃;
for 3h;
With
methanol; sodium tetrahydroborate;
In
ethanol; ethyl acetate;
at 0 ℃;
for 1h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: trimethylsilyl trifluoromethanesulfonate; DBN / acetonitrile / 21 h / 0 - 65 °C
2.1: sodium methylate / 24 h / 20 °C
3.1: pyridine / 16 h / 20 °C
4.1: pyridine / dichloromethane / 5 h / 20 °C
5.1: water; 4-methylmorpholine N-oxide / osmium(VIII) oxide / tert-butyl alcohol; tetrahydrofuran / 16 h / 20 °C
6.1: sodium periodate / water; tetrahydrofuran / 3 h / 20 °C
6.2: 1 h / 0 °C
With
pyridine; sodium periodate; trimethylsilyl trifluoromethanesulfonate; DBN; water; sodium methylate; 4-methylmorpholine N-oxide;
pyridine; osmium(VIII) oxide;
In
tetrahydrofuran; dichloromethane; water; acetonitrile; tert-butyl alcohol;