5-Chloro-2-methoxybenzenesulfonic acid hydrazide

Base Information

Chemical Name:5-Chloro-2-methoxybenzenesulfonic acid hydrazide
CAS No.:22952-33-6
Molecular Formula:C₇H₉ClN₂O₃S
Molecular Weight:236.679
Hs Code.:
DSSTox Substance ID:DTXSID201237105

Synonyms:5-Chloro-2-methoxybenzenesulfonic acid hydrazide;SCHEMBL419973;DTXSID201237105;22952-33-6

Suppliers and Price of 5-Chloro-2-methoxybenzenesulfonic acid hydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-Chloro-2-methoxybenzenesulfonic acid hydrazide

Chemical Property:

XLogP3:0.7
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:3
Exact Mass:236.0022410
Heavy Atom Count:14
Complexity:277

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=C(C=C(C=C1)Cl)S(=O)(=O)NN

Technology Process of 5-Chloro-2-methoxybenzenesulfonic acid hydrazide

There total 2 articles about 5-Chloro-2-methoxybenzenesulfonic acid hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 22952-32-5
5-chloro-2-methoxybenzenesulfonyl chloride

: 22952-33-6
5-chloro-2-methoxybenzenesulfonohydrazide

Guidance literature:: With hydrazine hydrate; In tetrahydrofuran; at 0 - 20 ℃;
DOI:10.1016/j.jfluchem.2013.01.033

Reference yield:

: 623-12-1
4-chloromethoxybenzene

: 22952-33-6
5-chloro-2-methoxybenzenesulfonohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: ClSO₃H

2: N₂H₄*H₂O

With chlorosulfonic acid; hydrazine hydrate;
DOI:10.1039/j39690001341