dimethylthexylsilyl O-(methyl 2-O-levulinoyl-3-O-benzyl-β-D-glucopyranosyluronate)-(1->4)-O-2-azido-3-O-benzyl-2-deoxy-6-O-levulinoyl-β-D-glucopyranoside

Base Information

• Chemical Name: dimethylthexylsilyl O-(methyl 2-O-levulinoyl-3-O-benzyl-β-D-glucopyranosyluronate)-(1->4)-O-2-azido-3-O-benzyl-2-deoxy-6-O-levulinoyl-β-D-glucopyranoside
• CAS No.: 1198156-27-2
• Molecular Formula: C₄₅H₆₃N₃O₁₅Si
• Molecular Weight: 914.092

Synonyms:dimethylthexylsilyl O-(methyl 2-O-levulinoyl-3-O-benzyl-β-D-glucopyranosyluronate)-(1->4)-O-2-azido-3-O-benzyl-2-deoxy-6-O-levulinoyl-β-D-glucopyranoside

Chemical Property of dimethylthexylsilyl O-(methyl 2-O-levulinoyl-3-O-benzyl-β-D-glucopyranosyluronate)-(1->4)-O-2-azido-3-O-benzyl-2-deoxy-6-O-levulinoyl-β-D-glucopyranoside

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Technology Process of dimethylthexylsilyl O-(methyl 2-O-levulinoyl-3-O-benzyl-β-D-glucopyranosyluronate)-(1->4)-O-2-azido-3-O-benzyl-2-deoxy-6-O-levulinoyl-β-D-glucopyranoside

There total 2 articles about dimethylthexylsilyl O-(methyl 2-O-levulinoyl-3-O-benzyl-β-D-glucopyranosyluronate)-(1->4)-O-2-azido-3-O-benzyl-2-deoxy-6-O-levulinoyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diazomethane (186581-53-3,908094-01-9,334-88-3) + C44H61N3O15Si → dimethylthexylsilyl O-(methyl 2-O-levulinoyl-3-O-benzyl-β-D-glucopyranosyluronate)-(1->4)-O-2-azido-3-O-benzyl-2-deoxy-6-O-levulinoyl-β-D-glucopyranoside (1198156-27-2)

Guidance literature:

In tetrahydrofuran; diethyl ether; at 20 ℃;

DOI:10.1021/ja907358k

Reference yield:

→ dimethylthexylsilyl O-(methyl 2-O-levulinoyl-3-O-benzyl-β-D-glucopyranosyluronate)-(1->4)-O-2-azido-3-O-benzyl-2-deoxy-6-O-levulinoyl-β-D-glucopyranoside (1198156-27-2)

Guidance literature:

Reference yield: 82.0%

dimethylthexylsilyl O-(methyl 2-O-levulinoyl-3-O-benzyl-β-D-glucopyranosyluronate)-(1->4)-O-2-azido-3-O-benzyl-2-deoxy-6-O-levulinoyl-β-D-glucopyranoside (1198156-27-2) + (fluorenylmethoxy)carbonyl chloride (28920-43-6) → dimethylthexylsilyl O-(methyl 2-O-levulinoyl-3-O-benzyl-4-O-(9-fluorenylmethoxycarbonyl)-β-D-glucopyranosyluronate)-(1->4)-O-2-azido-3-O-benzyl-2-deoxy-6-O-levulinoyl-β-D-glucopyranoside (1198155-93-9)

Guidance literature:

With pyridine; dmap; In dichloromethane; at 0 - 20 ℃;

DOI:10.1021/ja907358k

upstream raw materials:

diazomethane

Downstream raw materials:

dimethylthexylsilyl O-(methyl 2-O-levulinoyl-3-O-benzyl-4-O-(9-fluorenylmethoxycarbonyl)-β-D-glucopyranosyluronate)-(1->4)-O-2-azido-3-O-benzyl-2-deoxy-6-O-levulinoyl-β-D-glucopyranoside

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