1-phenyl-3-[(1E,3E)-4-phenyl-1,3-butadienyl]-5-[(E)-2-phenylethenyl]-1H-pyrazole

Base Information

• Chemical Name: 1-phenyl-3-[(1E,3E)-4-phenyl-1,3-butadienyl]-5-[(E)-2-phenylethenyl]-1H-pyrazole
• CAS No.: 904927-21-5
• Molecular Formula: C₂₇H₂₂N₂
• Molecular Weight: 374.485

Synonyms:1-phenyl-3-[(1E,3E)-4-phenyl-1,3-butadienyl]-5-[(E)-2-phenylethenyl]-1H-pyrazole

Chemical Property of 1-phenyl-3-[(1E,3E)-4-phenyl-1,3-butadienyl]-5-[(E)-2-phenylethenyl]-1H-pyrazole

Chemical Property:

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Technology Process of 1-phenyl-3-[(1E,3E)-4-phenyl-1,3-butadienyl]-5-[(E)-2-phenylethenyl]-1H-pyrazole

There total 3 articles about 1-phenyl-3-[(1E,3E)-4-phenyl-1,3-butadienyl]-5-[(E)-2-phenylethenyl]-1H-pyrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

1-phenyl-3-[(1E,3E)-4-phenyl-1,3-butadienyl]-5-[(E)-2-phenylethenyl]-4,5-dihydro-1H-pyrazole (904927-17-9) → 1-phenyl-3-[(1E,3E)-4-phenyl-1,3-butadienyl]-5-[(E)-2-phenylethenyl]-1H-pyrazole (904927-21-5)

Guidance literature:

With lead(IV) acetate; In dichloromethane; at 20 ℃; for 0.5h;

DOI:10.1007/s11178-006-0039-3

Reference yield:

dicinnamylideneacetone (622-21-9) → 1-phenyl-3-[(1E,3E)-4-phenyl-1,3-butadienyl]-5-[(E)-2-phenylethenyl]-1H-pyrazole (904927-21-5)

Guidance literature:

Multi-step reaction with 2 steps

1.1: acetic acid / 0.25 h / Heating

1.2: 19 percent / acetic acid; ethanol / 0.5 h / Heating

2.1: 71 percent / lead tetraacetate / CH₂Cl₂ / 0.5 h / 20 °C

With lead(IV) acetate; In dichloromethane; acetic acid;

DOI:10.1007/s11178-006-0039-3

Reference yield:

phenylhydrazine (100-63-0) → 1-phenyl-3-[(1E,3E)-4-phenyl-1,3-butadienyl]-5-[(E)-2-phenylethenyl]-1H-pyrazole (904927-21-5)

Guidance literature:

Multi-step reaction with 2 steps

1.1: acetic acid / 0.25 h / Heating

1.2: 19 percent / acetic acid; ethanol / 0.5 h / Heating

2.1: 71 percent / lead tetraacetate / CH₂Cl₂ / 0.5 h / 20 °C

With lead(IV) acetate; In dichloromethane; acetic acid;

DOI:10.1007/s11178-006-0039-3

upstream raw materials:

1-phenyl-3-[(1E,3E)-4-phenyl-1,3-butadienyl]-5-[(E)-2-phenylethenyl]-4,5-dihydro-1H-pyrazole

dicinnamylideneacetone

phenylhydrazine

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