(3R,4R,6R,7R)-3,7-Dibenzyloxy-4-(tert-butyldimethylsiloxy)-8,8-diethylthio-6-(p-methoxybenzyloxy)-5,5-dimethyl-2-(trimethylsiloxy)octene

Base Information

• Chemical Name: (3R,4R,6R,7R)-3,7-Dibenzyloxy-4-(tert-butyldimethylsiloxy)-8,8-diethylthio-6-(p-methoxybenzyloxy)-5,5-dimethyl-2-(trimethylsiloxy)octene
• CAS No.: 163226-85-5
• Molecular Formula: C₄₅H₇₀O₆S₂Si₂
• Molecular Weight: 827.35

Synonyms:(3R,4R,6R,7R)-3,7-Dibenzyloxy-4-(tert-butyldimethylsiloxy)-8,8-diethylthio-6-(p-methoxybenzyloxy)-5,5-dimethyl-2-(trimethylsiloxy)octene

Chemical Property of (3R,4R,6R,7R)-3,7-Dibenzyloxy-4-(tert-butyldimethylsiloxy)-8,8-diethylthio-6-(p-methoxybenzyloxy)-5,5-dimethyl-2-(trimethylsiloxy)octene

Chemical Property:

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Technology Process of (3R,4R,6R,7R)-3,7-Dibenzyloxy-4-(tert-butyldimethylsiloxy)-8,8-diethylthio-6-(p-methoxybenzyloxy)-5,5-dimethyl-2-(trimethylsiloxy)octene

There total 1 articles about (3R,4R,6R,7R)-3,7-Dibenzyloxy-4-(tert-butyldimethylsiloxy)-8,8-diethylthio-6-(p-methoxybenzyloxy)-5,5-dimethyl-2-(trimethylsiloxy)octene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

chloro-trimethyl-silane (75-77-4) + (3R,4R,6R,7R)-3,7-Dibenzyloxy-4-(tert-butyldimethylsiloxy)-8,8-diethylthio-6-(p-methoxybenzyloxy)-5,5-dimethyl-2-octanone → (3R,4R,6R,7R)-3,7-Dibenzyloxy-4-(tert-butyldimethylsiloxy)-8,8-diethylthio-6-(p-methoxybenzyloxy)-5,5-dimethyl-2-(trimethylsiloxy)octene (163226-85-5)

Guidance literature:

With lithium diisopropyl amide; In tetrahydrofuran; at -78 - 20 ℃;

DOI:10.1246/cl.1995.181

Reference yield: 78.0%

(3R,4R,6R,7R)-3,7-Dibenzyloxy-4-(tert-butyldimethylsiloxy)-8,8-diethylthio-6-(p-methoxybenzyloxy)-5,5-dimethyl-2-(trimethylsiloxy)octene (163226-85-5) + (3R,4R,6R,7R)-3,7-Bis-benzyloxy-4-(tert-butyl-dimethyl-silanyloxy)-6-(4-methoxy-benzyloxy)-5,5-dimethyl-8-phenylsulfanyl-8-trimethylsilanyloxy-octan-2-one (163226-84-4) → 1-[(1R,3R,4R)-4-Benzyloxy-1-((R)-1-benzyloxy-2-phenylsulfanyl-2-trimethylsilanyloxy-ethyl)-3-(tert-butyl-dimethyl-silanyloxy)-2,2-dimethyl-5-trimethylsilanyloxy-hex-5-enyloxymethyl]-4-methoxy-benzene

Guidance literature:

With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 - 20 ℃;

DOI:10.1246/cl.1995.181

Reference yield: 57.0%

(3R,4R,6R,7R)-3,7-Dibenzyloxy-4-(tert-butyldimethylsiloxy)-8,8-diethylthio-6-(p-methoxybenzyloxy)-5,5-dimethyl-2-(trimethylsiloxy)octene (163226-85-5) → (2R,3R)-3-Benzyloxy-2-[(2R,3R)-3-benzyloxy-2-(tert-butyl-dimethyl-silanyloxy)-4-ethylsulfanyl-1,1-dimethyl-butyl]-6-(4-methoxy-phenyl)-tetrahydro-pyran-4-one

Guidance literature:

With tris(trimethylsilyl)amine; Cl⁽³⁾HO₄; In dichloromethane; at -78 ℃;

DOI:10.1246/cl.1995.181

upstream raw materials:

chloro-trimethyl-silane

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