(E)-1-[2-(3,3-diisopropyltriaz-1-enyl)-3-(trifluoromethyl)phenyl]ethanone

Base Information

Chemical Name:(E)-1-[2-(3,3-diisopropyltriaz-1-enyl)-3-(trifluoromethyl)phenyl]ethanone
CAS No.:1052092-85-9
Molecular Formula:C₁₅H₂₀F₃N₃O
Molecular Weight:315.339
Hs Code.:

Synonyms:(E)-1-[2-(3,3-diisopropyltriaz-1-enyl)-3-(trifluoromethyl)phenyl]ethanone

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Chemical Property of (E)-1-[2-(3,3-diisopropyltriaz-1-enyl)-3-(trifluoromethyl)phenyl]ethanone

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Technology Process of (E)-1-[2-(3,3-diisopropyltriaz-1-enyl)-3-(trifluoromethyl)phenyl]ethanone

There total 2 articles about (E)-1-[2-(3,3-diisopropyltriaz-1-enyl)-3-(trifluoromethyl)phenyl]ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1052092-62-2
(E)-2-(3,3-diisopropyltriaz-1-enyl)-3-(trifluoromethyl)benzonitrile

: 75-16-1
methylmagnesium bromide

: 1052092-85-9
(E)-1-[2-(3,3-diisopropyltriaz-1-enyl)-3-(trifluoromethyl)phenyl]ethanone

Guidance literature:: (E)-2-(3,3-diisopropyltriaz-1-enyl)-3-(trifluoromethyl)benzonitrile; methylmagnesium bromide; In tetrahydrofuran; diethyl ether; at 20 ℃; for 3h; Inert atmosphere;

With silica gel; In diethyl ether; pentane; Column chromatography;
DOI:10.1002/ejoc.200800154

Reference yield: 78.0%

: 1052092-62-2
(E)-2-(3,3-diisopropyltriaz-1-enyl)-3-(trifluoromethyl)benzonitrile

: 917-54-4
methyllithium

: 1052092-85-9
(E)-1-[2-(3,3-diisopropyltriaz-1-enyl)-3-(trifluoromethyl)phenyl]ethanone

Guidance literature:: (E)-2-(3,3-diisopropyltriaz-1-enyl)-3-(trifluoromethyl)benzonitrile; methyllithium; In tetrahydrofuran; diethyl ether; at 0 - 20 ℃; Inert atmosphere;

With silica gel; In diethyl ether; pentane; Column chromatography;
DOI:10.1002/ejoc.200800154

Reference yield: 57.0%

: 1052092-85-9
(E)-1-[2-(3,3-diisopropyltriaz-1-enyl)-3-(trifluoromethyl)phenyl]ethanone

: 1052093-03-4
(E)-1-[2-(3,3-diisopropyltriaz-1-enyl)-3-(trifluoromethyl)phenyl]ethanamine

Guidance literature:: (E)-1-[2-(3,3-diisopropyltriaz-1-enyl)-3-(trifluoromethyl)phenyl]ethanone; With ammonia; titanium(IV)isopropoxide; In methanol; at 50 ℃; for 6h; Inert atmosphere;

With methanol; lithium borohydride; In tetrahydrofuran; at 0 ℃; for 3h; Inert atmosphere;
DOI:10.1002/ejoc.200800154