3-{4-[(2-butyl-5-methanesulfonamide-1-benzofuran-3-yl)carbonyl]phenoxy}propyl methanesulfonate

Base Information

Chemical Name:3-{4-[(2-butyl-5-methanesulfonamide-1-benzofuran-3-yl)carbonyl]phenoxy}propyl methanesulfonate
CAS No.:1310430-09-1
Molecular Formula:C₂₄H₂₉NO₈S₂
Molecular Weight:523.628
Hs Code.:

Synonyms:3-{4-[(2-butyl-5-methanesulfonamide-1-benzofuran-3-yl)carbonyl]phenoxy}propyl methanesulfonate

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Chemical Property of 3-{4-[(2-butyl-5-methanesulfonamide-1-benzofuran-3-yl)carbonyl]phenoxy}propyl methanesulfonate

Chemical Property:

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Technology Process of 3-{4-[(2-butyl-5-methanesulfonamide-1-benzofuran-3-yl)carbonyl]phenoxy}propyl methanesulfonate

There total 3 articles about 3-{4-[(2-butyl-5-methanesulfonamide-1-benzofuran-3-yl)carbonyl]phenoxy}propyl methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1310430-13-7
3-{4-[(5-amino-2-butyl-1-benzofuran-3-yl)carbonyl]phenoxy}propan-1-ol

: 124-63-0
methanesulfonyl chloride

: 1310430-09-1
3-{4-[(2-butyl-5-methanesulfonamide-1-benzofuran-3-yl)carbonyl]phenoxy}propyl methanesulfonate

Guidance literature:: With pyridine; In dichloromethane; at 10 - 20 ℃; for 24h;

Reference yield:

: 141645-16-1
2-n-butyl-3-(4-hydroxybenzoyl)-5-nitrobenzofuran

: 1310430-09-1
3-{4-[(2-butyl-5-methanesulfonamide-1-benzofuran-3-yl)carbonyl]phenoxy}propyl methanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate; potassium iodide; tetrabutylammomium bromide / N,N-dimethyl-formamide / 0.5 h / 50 °C

1.2: 80 - 85 °C

2.1: hydrogen / palladium 10% on activated carbon / water; methanol / 40 °C / 3000.3 Torr / Autoclave

3.1: pyridine / dichloromethane / 24 h / 10 - 20 °C

With pyridine; tetrabutylammomium bromide; hydrogen; potassium carbonate; potassium iodide; palladium 10% on activated carbon; In methanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 1310430-11-5
3-{ 4-[(2-butyl-5-nitro-1-benzofuran-3-yl) carbonyl]phenoxy}propan-1-ol

: 1310430-09-1
3-{4-[(2-butyl-5-methanesulfonamide-1-benzofuran-3-yl)carbonyl]phenoxy}propyl methanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / palladium 10% on activated carbon / water; methanol / 40 °C / 3000.3 Torr / Autoclave

2: pyridine / dichloromethane / 24 h / 10 - 20 °C

With pyridine; hydrogen; palladium 10% on activated carbon; In methanol; dichloromethane; water;